Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization

Ultrasound assisted extraction (UAE) was evaluated as a green procedure for the recovery of phenolic compounds with antioxidant capacity from underutilized mango ’criollo’ (peel, pulp and seed). Magnetic stirred was performed as conventional extraction. Response surface methodology using a three-fac...

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Autores principales: Ojeda, Gonzalo Adrián, Sgroppo, Sonia Cecilia, Sánchez Moreno, Concepción, De Ancos, Begoña
Formato: Artículo
Lenguaje:Inglés
Publicado: Elsevier 2025
Materias:
Polyphenols
Quercetin derivatives
Mangiferin
RSM
HPLC-MS/MS
Acceso en línea:http://repositorio.unne.edu.ar/handle/123456789/59132
Aporte de:
RIUNNE - Repositorio Institucional de la Universidad Nacional del Nordeste (UNNE) de Universidad Nacional del Nordeste
id I48-R184-123456789-59132
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spelling I48-R184-123456789-591322025-12-05T11:19:49Z Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization Ojeda, Gonzalo Adrián Sgroppo, Sonia Cecilia Sánchez Moreno, Concepción De Ancos, Begoña Polyphenols Quercetin derivatives Mangiferin RSM HPLC-MS/MS Ultrasound assisted extraction (UAE) was evaluated as a green procedure for the recovery of phenolic compounds with antioxidant capacity from underutilized mango ’criollo’ (peel, pulp and seed). Magnetic stirred was performed as conventional extraction. Response surface methodology using a three-factor (% ethanol, amplitude and time) central composite design was used to maximize the extraction for total phenolic compounds (TPC), total flavonoids and antioxidant capacity. The operational conditions to maximize extraction were: peel, 46% ethanol/amplitude 60% (36 μm)/6.5 min; pulp, 25% ethanol/amplitude 75% (45 μm)/30 min; seed 49% ethanol/100% (60 μm) amplitude/20 min. The phenolic composition of the optimized extracts was characterized by HPLC-QTOF-MS/MS and 45 compounds were tentatively identified as xanthones (mangiferin), flavonoids (quercetin), ellagic acid, benzophenones (maclurin), gallate derivatives and gallotannins. UAE increased TPC extraction (33%); interestingly mangiferin extraction increased 53% in peel, similarly, ellagic acid increased up to 2.5 and 4.4 times in peel and seed extracts. 2025-12-05T11:11:37Z 2025-12-05T11:11:37Z 2022-12-01 Artículo Ojeda, Gonzalo Adrián, et al., 2022. Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization. Food Chemistry. Ámsterdam: Países Bajos, vol. 396, p. 1-13. E-ISSN 2772-753X. DOI https://doi.org/10.1016/j.foodchem.2022.133738 http://repositorio.unne.edu.ar/handle/123456789/59132 en https://doi.org/10.1016/j.foodchem.2022.133738 restrictedAccess http://creativecommons.org/licenses/by-nc-nd/2.5/ar/ application/pdf p. 1-13 application/pdf Elsevier Food Chemistry, 2022, vol. 396, p. 1-13.
institution Universidad Nacional del Nordeste
institution_str I-48
repository_str R-184
collection RIUNNE - Repositorio Institucional de la Universidad Nacional del Nordeste (UNNE)
language Inglés
topic Polyphenols
Quercetin derivatives
Mangiferin
RSM
HPLC-MS/MS
spellingShingle Polyphenols
Quercetin derivatives
Mangiferin
RSM
HPLC-MS/MS
Ojeda, Gonzalo Adrián
Sgroppo, Sonia Cecilia
Sánchez Moreno, Concepción
De Ancos, Begoña
Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization
topic_facet Polyphenols
Quercetin derivatives
Mangiferin
RSM
HPLC-MS/MS
description Ultrasound assisted extraction (UAE) was evaluated as a green procedure for the recovery of phenolic compounds with antioxidant capacity from underutilized mango ’criollo’ (peel, pulp and seed). Magnetic stirred was performed as conventional extraction. Response surface methodology using a three-factor (% ethanol, amplitude and time) central composite design was used to maximize the extraction for total phenolic compounds (TPC), total flavonoids and antioxidant capacity. The operational conditions to maximize extraction were: peel, 46% ethanol/amplitude 60% (36 μm)/6.5 min; pulp, 25% ethanol/amplitude 75% (45 μm)/30 min; seed 49% ethanol/100% (60 μm) amplitude/20 min. The phenolic composition of the optimized extracts was characterized by HPLC-QTOF-MS/MS and 45 compounds were tentatively identified as xanthones (mangiferin), flavonoids (quercetin), ellagic acid, benzophenones (maclurin), gallate derivatives and gallotannins. UAE increased TPC extraction (33%); interestingly mangiferin extraction increased 53% in peel, similarly, ellagic acid increased up to 2.5 and 4.4 times in peel and seed extracts.
format Artículo
author Ojeda, Gonzalo Adrián
Sgroppo, Sonia Cecilia
Sánchez Moreno, Concepción
De Ancos, Begoña
author_facet Ojeda, Gonzalo Adrián
Sgroppo, Sonia Cecilia
Sánchez Moreno, Concepción
De Ancos, Begoña
author_sort Ojeda, Gonzalo Adrián
title Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization
title_short Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization
title_full Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization
title_fullStr Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization
title_full_unstemmed Mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. Ultrasound assisted extraction evaluated by response surface methodology and HPLC-ESI-QTOF-MS/MS characterization
title_sort mango ‘criollo’ by-products as a source of polyphenols with antioxidant capacity. ultrasound assisted extraction evaluated by response surface methodology and hplc-esi-qtof-ms/ms characterization
publisher Elsevier
publishDate 2025
url http://repositorio.unne.edu.ar/handle/123456789/59132
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