Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy

An optical noncontact technique is presented that provides a two-dimensional map of the hardness of treated steel at the micrometer level. The photodeflection technique for determining the thermal diffusivity is shown to be a useful and rapid way to determine the hardness increase profile in two dim...

Descripción completa

Guardado en:
Detalles Bibliográficos
Autores principales: Archiopoli, U.C., Mingolo, N., Martínez, O.E.
Formato: JOUR
Materias:
Acceso en línea:http://hdl.handle.net/20.500.12110/paper_02578972_v205_n8-9_p3087_Archiopoli
Aporte de:
id todo:paper_02578972_v205_n8-9_p3087_Archiopoli
record_format dspace
spelling todo:paper_02578972_v205_n8-9_p3087_Archiopoli2023-10-03T15:11:40Z Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy Archiopoli, U.C. Mingolo, N. Martínez, O.E. Hardness Surface characterization Thermal diffusivity After-treatment Anomalous regions Diffusivities Micrometer levels Non-contact techniques Phase delay Photodeflection technique Photothermal deflections Pump beams Strong correlation Surface characterization Two dimensional mapping Two-dimension Two-dimensional map Hardness Scanning electron microscopy Surface properties Thermal diffusion Thermal diffusivity Two dimensional An optical noncontact technique is presented that provides a two-dimensional map of the hardness of treated steel at the micrometer level. The photodeflection technique for determining the thermal diffusivity is shown to be a useful and rapid way to determine the hardness increase profile in two dimensions with only minor preparation of the sample (flat polish). This is possible due to the strong correlation found for this type of material between the inverse of the diffusivity and the hardness increment after treatment. The diffusivity retrieval is performed by a single measurement of the phase delay between the pump beam and the photodeflection signal thus allowing a rapid scanning of the surface. The surface scans of the hardness performed with this technique showed that anomalous regions can be identified that direct optical or scanning electron microscopy observation do not reveal. © 2010 Elsevier B.V. JOUR info:eu-repo/semantics/openAccess http://creativecommons.org/licenses/by/2.5/ar http://hdl.handle.net/20.500.12110/paper_02578972_v205_n8-9_p3087_Archiopoli
institution Universidad de Buenos Aires
institution_str I-28
repository_str R-134
collection Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA)
topic Hardness
Surface characterization
Thermal diffusivity
After-treatment
Anomalous regions
Diffusivities
Micrometer levels
Non-contact techniques
Phase delay
Photodeflection technique
Photothermal deflections
Pump beams
Strong correlation
Surface characterization
Two dimensional mapping
Two-dimension
Two-dimensional map
Hardness
Scanning electron microscopy
Surface properties
Thermal diffusion
Thermal diffusivity
Two dimensional
spellingShingle Hardness
Surface characterization
Thermal diffusivity
After-treatment
Anomalous regions
Diffusivities
Micrometer levels
Non-contact techniques
Phase delay
Photodeflection technique
Photothermal deflections
Pump beams
Strong correlation
Surface characterization
Two dimensional mapping
Two-dimension
Two-dimensional map
Hardness
Scanning electron microscopy
Surface properties
Thermal diffusion
Thermal diffusivity
Two dimensional
Archiopoli, U.C.
Mingolo, N.
Martínez, O.E.
Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy
topic_facet Hardness
Surface characterization
Thermal diffusivity
After-treatment
Anomalous regions
Diffusivities
Micrometer levels
Non-contact techniques
Phase delay
Photodeflection technique
Photothermal deflections
Pump beams
Strong correlation
Surface characterization
Two dimensional mapping
Two-dimension
Two-dimensional map
Hardness
Scanning electron microscopy
Surface properties
Thermal diffusion
Thermal diffusivity
Two dimensional
description An optical noncontact technique is presented that provides a two-dimensional map of the hardness of treated steel at the micrometer level. The photodeflection technique for determining the thermal diffusivity is shown to be a useful and rapid way to determine the hardness increase profile in two dimensions with only minor preparation of the sample (flat polish). This is possible due to the strong correlation found for this type of material between the inverse of the diffusivity and the hardness increment after treatment. The diffusivity retrieval is performed by a single measurement of the phase delay between the pump beam and the photodeflection signal thus allowing a rapid scanning of the surface. The surface scans of the hardness performed with this technique showed that anomalous regions can be identified that direct optical or scanning electron microscopy observation do not reveal. © 2010 Elsevier B.V.
format JOUR
author Archiopoli, U.C.
Mingolo, N.
Martínez, O.E.
author_facet Archiopoli, U.C.
Mingolo, N.
Martínez, O.E.
author_sort Archiopoli, U.C.
title Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy
title_short Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy
title_full Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy
title_fullStr Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy
title_full_unstemmed Two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy
title_sort two-dimensional mapping of micro-hardness increase on surface treated steel determined by photothermal deflection microscopy
url http://hdl.handle.net/20.500.12110/paper_02578972_v205_n8-9_p3087_Archiopoli
work_keys_str_mv AT archiopoliuc twodimensionalmappingofmicrohardnessincreaseonsurfacetreatedsteeldeterminedbyphotothermaldeflectionmicroscopy
AT mingolon twodimensionalmappingofmicrohardnessincreaseonsurfacetreatedsteeldeterminedbyphotothermaldeflectionmicroscopy
AT martinezoe twodimensionalmappingofmicrohardnessincreaseonsurfacetreatedsteeldeterminedbyphotothermaldeflectionmicroscopy
_version_ 1782028283198570496