Synthesis of cholesterol‐20‐14C
Cholesterol‐20‐14C was synthesized in four steps from pregnenolone‐20‐14C. The labelled intermediates were proven to be cholest‐5‐ene‐3β, 20α‐diol acetate‐3, cholesta‐5, 20 (22)‐diene‐3β‐ol acetate, and cholesterol acetate by 1H‐n.m.r. spectroscopical analysis. Cholesterol‐20‐14C was obtained with a...
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todo:paper_00222135_v6_n4_p369_Porto2023-10-03T14:28:31Z Synthesis of cholesterol‐20‐14C Porto, A.M. Gros, E.G. Cholesterol‐20‐14C was synthesized in four steps from pregnenolone‐20‐14C. The labelled intermediates were proven to be cholest‐5‐ene‐3β, 20α‐diol acetate‐3, cholesta‐5, 20 (22)‐diene‐3β‐ol acetate, and cholesterol acetate by 1H‐n.m.r. spectroscopical analysis. Cholesterol‐20‐14C was obtained with a radiochemical purity exceeding 99%. Copyright © 1970 John Wiley & Sons, Ltd. Fil:Porto, A.M. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil:Gros, E.G. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. JOUR info:eu-repo/semantics/openAccess http://creativecommons.org/licenses/by/2.5/ar http://hdl.handle.net/20.500.12110/paper_00222135_v6_n4_p369_Porto |
institution |
Universidad de Buenos Aires |
institution_str |
I-28 |
repository_str |
R-134 |
collection |
Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA) |
description |
Cholesterol‐20‐14C was synthesized in four steps from pregnenolone‐20‐14C. The labelled intermediates were proven to be cholest‐5‐ene‐3β, 20α‐diol acetate‐3, cholesta‐5, 20 (22)‐diene‐3β‐ol acetate, and cholesterol acetate by 1H‐n.m.r. spectroscopical analysis. Cholesterol‐20‐14C was obtained with a radiochemical purity exceeding 99%. Copyright © 1970 John Wiley & Sons, Ltd. |
format |
JOUR |
author |
Porto, A.M. Gros, E.G. |
spellingShingle |
Porto, A.M. Gros, E.G. Synthesis of cholesterol‐20‐14C |
author_facet |
Porto, A.M. Gros, E.G. |
author_sort |
Porto, A.M. |
title |
Synthesis of cholesterol‐20‐14C |
title_short |
Synthesis of cholesterol‐20‐14C |
title_full |
Synthesis of cholesterol‐20‐14C |
title_fullStr |
Synthesis of cholesterol‐20‐14C |
title_full_unstemmed |
Synthesis of cholesterol‐20‐14C |
title_sort |
synthesis of cholesterol‐20‐14c |
url |
http://hdl.handle.net/20.500.12110/paper_00222135_v6_n4_p369_Porto |
work_keys_str_mv |
AT portoam synthesisofcholesterol2014c AT groseg synthesisofcholesterol2014c |
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1782023774155046912 |