Thin-layer chromatography of acyl derivatives of sugars

Acyl derivatives of sugars have been separated and characterised by thin-layer chromatography. We consider this method of great value for the resolution and identification of a mixture of anomers. Separation was completed within 20 minutes, with benzene alone or mixed with more polar solvents. In al...

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Autores principales: Deferrari, J.O., de Lederkremer, R.M., Matsuhiro, B., Sproviero, J.F.
Formato: JOUR
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Acceso en línea:http://hdl.handle.net/20.500.12110/paper_00219673_v9_nC_p283_Deferrari
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Sumario:Acyl derivatives of sugars have been separated and characterised by thin-layer chromatography. We consider this method of great value for the resolution and identification of a mixture of anomers. Separation was completed within 20 minutes, with benzene alone or mixed with more polar solvents. In all cases the acyl derivative with a 1,5-trans configuration had a higher RF value than the respective anomer, with the exception of d-glycero-d-gulo-heptose. © 1962.