Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces

Silica nanoparticles were surface-functionalized with diazonium groups. The reaction steps leading to the formation of the diazonium functionality were followed with IR and XPS, and the structure of the diazonium-functionalized nanoparticle was confirmed with solid state NMR. Nanoparticle size distr...

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Detalles Bibliográficos
Autores principales:	Joselevich, María, Williams, Federico Jose
Publicado:	2008
Materias:	Gold deposits Nanoparticles Nanostructured materials Nuclear magnetic resonance Secondary emission Silica Size distribution Covalent attachments Covalently bonded Functionalized Functionalized nanoparticles Iron surfaces Metal surfaces Nanoparticle size distributions Reaction steps Silica nanoparticles Solid state nmr Spatial distributions Synthesis and characterizations Nanostructures
Acceso en línea:	https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_07437463_v24_n20_p11711_Joselevich http://hdl.handle.net/20.500.12110/paper_07437463_v24_n20_p11711_Joselevich
Aporte de:	Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA) de Universidad de Buenos Aires

id	paper:paper_07437463_v24_n20_p11711_Joselevich
record_format	dspace
spelling	paper:paper_07437463_v24_n20_p11711_Joselevich2023-06-08T15:44:55Z Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces Joselevich, María Williams, Federico Jose Gold deposits Nanoparticles Nanostructured materials Nuclear magnetic resonance Secondary emission Silica Size distribution Covalent attachments Covalently bonded Functionalized Functionalized nanoparticles Iron surfaces Metal surfaces Nanoparticle size distributions Reaction steps Silica nanoparticles Solid state nmr Spatial distributions Synthesis and characterizations Nanostructures Silica nanoparticles were surface-functionalized with diazonium groups. The reaction steps leading to the formation of the diazonium functionality were followed with IR and XPS, and the structure of the diazonium-functionalized nanoparticle was confirmed with solid state NMR. Nanoparticle size distribution was determined with DLS, SEM, and TEM. The nanoparticles were then covalently bonded to gold and iron surfaces. Their spatial distribution over the metal surface was analyzed by SEM. Diazonium modification of nanoparticles represents a new method for the covalent attachment of nanoparticles to metal surfaces. © 2008 American Chemical Society. Fil:Joselevich, M. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil:Williams, F.J. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. 2008 https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_07437463_v24_n20_p11711_Joselevich http://hdl.handle.net/20.500.12110/paper_07437463_v24_n20_p11711_Joselevich
institution	Universidad de Buenos Aires
institution_str	I-28
repository_str	R-134
collection	Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA)
topic	Gold deposits Nanoparticles Nanostructured materials Nuclear magnetic resonance Secondary emission Silica Size distribution Covalent attachments Covalently bonded Functionalized Functionalized nanoparticles Iron surfaces Metal surfaces Nanoparticle size distributions Reaction steps Silica nanoparticles Solid state nmr Spatial distributions Synthesis and characterizations Nanostructures
spellingShingle	Gold deposits Nanoparticles Nanostructured materials Nuclear magnetic resonance Secondary emission Silica Size distribution Covalent attachments Covalently bonded Functionalized Functionalized nanoparticles Iron surfaces Metal surfaces Nanoparticle size distributions Reaction steps Silica nanoparticles Solid state nmr Spatial distributions Synthesis and characterizations Nanostructures Joselevich, María Williams, Federico Jose Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces
topic_facet	Gold deposits Nanoparticles Nanostructured materials Nuclear magnetic resonance Secondary emission Silica Size distribution Covalent attachments Covalently bonded Functionalized Functionalized nanoparticles Iron surfaces Metal surfaces Nanoparticle size distributions Reaction steps Silica nanoparticles Solid state nmr Spatial distributions Synthesis and characterizations Nanostructures
description	Silica nanoparticles were surface-functionalized with diazonium groups. The reaction steps leading to the formation of the diazonium functionality were followed with IR and XPS, and the structure of the diazonium-functionalized nanoparticle was confirmed with solid state NMR. Nanoparticle size distribution was determined with DLS, SEM, and TEM. The nanoparticles were then covalently bonded to gold and iron surfaces. Their spatial distribution over the metal surface was analyzed by SEM. Diazonium modification of nanoparticles represents a new method for the covalent attachment of nanoparticles to metal surfaces. © 2008 American Chemical Society.
author	Joselevich, María Williams, Federico Jose
author_facet	Joselevich, María Williams, Federico Jose
author_sort	Joselevich, María
title	Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces
title_short	Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces
title_full	Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces
title_fullStr	Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces
title_full_unstemmed	Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces
title_sort	synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces
publishDate	2008
url	https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_07437463_v24_n20_p11711_Joselevich http://hdl.handle.net/20.500.12110/paper_07437463_v24_n20_p11711_Joselevich
work_keys_str_mv	AT joselevichmaria synthesisandcharacterizationofdiazoniumfunctionalizednanoparticlesfordepositiononmetalsurfaces AT williamsfedericojose synthesisandcharacterizationofdiazoniumfunctionalizednanoparticlesfordepositiononmetalsurfaces
_version_	1768542462377197568

Synthesis and characterization of diazonium functionalized nanoparticles for deposition on metal surfaces

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