Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds

3β-Hydroxy-5-cholenic acid was synthesized from 3β-hydroxy-5-pregnen-20-one in nine steps. The procedure would permit the labelling of C-22, C-23, and/or C-24 of the bile-acid side chain by choice of the appropriate labelled reagent. © 1977.

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Detalles Bibliográficos
Autores principales:	Burton, Gerardo, Gros, Eduardo Gervasio
Publicado:	1977
Materias:	carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols
Acceso en línea:	https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00224731_v8_n1_p69_Burton http://hdl.handle.net/20.500.12110/paper_00224731_v8_n1_p69_Burton
Aporte de:	Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA) de Universidad de Buenos Aires

id	paper:paper_00224731_v8_n1_p69_Burton
record_format	dspace
spelling	paper:paper_00224731_v8_n1_p69_Burton2023-06-08T14:51:06Z Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds Burton, Gerardo Gros, Eduardo Gervasio carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols 3β-Hydroxy-5-cholenic acid was synthesized from 3β-hydroxy-5-pregnen-20-one in nine steps. The procedure would permit the labelling of C-22, C-23, and/or C-24 of the bile-acid side chain by choice of the appropriate labelled reagent. © 1977. Fil:Burton, G. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil:Gros, E.G. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. 1977 https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00224731_v8_n1_p69_Burton http://hdl.handle.net/20.500.12110/paper_00224731_v8_n1_p69_Burton
institution	Universidad de Buenos Aires
institution_str	I-28
repository_str	R-134
collection	Biblioteca Digital - Facultad de Ciencias Exactas y Naturales (UBA)
topic	carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols
spellingShingle	carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols Burton, Gerardo Gros, Eduardo Gervasio Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
topic_facet	carbon cholane derivative pregnenolone sterol radioisotope article infrared spectrophotometry isotope labeling methodology nuclear magnetic resonance spectroscopy optical rotation synthesis 3beta hydroxycholenic acid in vitro study steroidogenesis theoretical study Carbon Radioisotopes Cholenes Isotope Labeling Magnetic Resonance Spectroscopy Optical Rotation Pregnenolone Spectrophotometry, Infrared Sterols
description	3β-Hydroxy-5-cholenic acid was synthesized from 3β-hydroxy-5-pregnen-20-one in nine steps. The procedure would permit the labelling of C-22, C-23, and/or C-24 of the bile-acid side chain by choice of the appropriate labelled reagent. © 1977.
author	Burton, Gerardo Gros, Eduardo Gervasio
author_facet	Burton, Gerardo Gros, Eduardo Gervasio
author_sort	Burton, Gerardo
title	Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
title_short	Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
title_full	Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
title_fullStr	Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
title_full_unstemmed	Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
title_sort	synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds
publishDate	1977
url	https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00224731_v8_n1_p69_Burton http://hdl.handle.net/20.500.12110/paper_00224731_v8_n1_p69_Burton
work_keys_str_mv	AT burtongerardo synthesisof3bhydroxy5cholenicacidfrom3bhydroxy5pregnen20oneaimedatthepreparationoflabelledsteroidcompounds AT groseduardogervasio synthesisof3bhydroxy5cholenicacidfrom3bhydroxy5pregnen20oneaimedatthepreparationoflabelledsteroidcompounds
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Synthesis of 3β-hydroxy-5-cholenic acid from 3β-hydroxy-5-pregnen-20-one aimed at the preparation of labelled steroid compounds

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