Prussian blue analogs: electrosynthesis and characterization

This article focuses on the electrodeposition and in situ characterization of Prussian blue analogs with the generic formula: AMk[Fe(CN)d i-mHf), where h, k, I, m are stoichiometric numbers, A = alkali metal cation, and M is a transitionmetal. Six such metal hexacyanoferrate (MHCF) compounds derived...

Descripción completa

Guardado en:
Detalles Bibliográficos
Autores principales: Lezna, Reynaldo Oscar, Tacconi, Norma R. de
Formato: Articulo
Lenguaje:Inglés
Publicado: 2003
Materias:
Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/167219
Aporte de:
Descripción
Sumario:This article focuses on the electrodeposition and in situ characterization of Prussian blue analogs with the generic formula: AMk[Fe(CN)d i-mHf), where h, k, I, m are stoichiometric numbers, A = alkali metal cation, and M is a transitionmetal. Six such metal hexacyanoferrate (MHCF) compounds derived from Cu, Pd, In, V, Co and Ni are featured in this article. The electrodeposition of MHCF films on targeted substrates is discussed through data obtained by cyclic voltammetry and complementan’ techniques. In situ spectroelectrochemical characterization of these films in the infrared and UV-visible regions is then discussed and constitutes the main topic of this article.