Retention in multistep programmed-temperature gas chromatography and flow control : Linear head pressure programs

A comparative study of retention in different systems of flow control that provide linear dependence with the temperature of the column's head pressure is performed by numerical simulation considering multistep (or multiramp) PTGC (programmed-temperature gas chromatography) as the most general...

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Autores principales: González, Francisco R., Nardillo, Ángel Miguel
Formato: Articulo
Lenguaje:Inglés
Publicado: 1997
Materias:
Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/123129
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id I19-R120-10915-123129
record_format dspace
institution Universidad Nacional de La Plata
institution_str I-19
repository_str R-120
collection SEDICI (UNLP)
language Inglés
topic Ciencias Exactas
temperature programming
head pressure
flow control systems
spellingShingle Ciencias Exactas
temperature programming
head pressure
flow control systems
González, Francisco R.
Nardillo, Ángel Miguel
Retention in multistep programmed-temperature gas chromatography and flow control : Linear head pressure programs
topic_facet Ciencias Exactas
temperature programming
head pressure
flow control systems
description A comparative study of retention in different systems of flow control that provide linear dependence with the temperature of the column's head pressure is performed by numerical simulation considering multistep (or multiramp) PTGC (programmed-temperature gas chromatography) as the most general situation. Calculation algorithms for each flow control mode are developed on the basis of a general retention equation and the only additional hypothesis is that certain geometric parameters of the column remain practically constant along the program. Procedures are individually contrasted with experiment, prior to application. The comparative view indicates that simple correlations cannot be obtained between retention times and temperatures in two different pressure controls or pressure programs. It seems that numerical procedures are unavoidable when it is required to convert the retention data from one chromatographic system to another with the same stationary phase.
format Articulo
Articulo
author González, Francisco R.
Nardillo, Ángel Miguel
author_facet González, Francisco R.
Nardillo, Ángel Miguel
author_sort González, Francisco R.
title Retention in multistep programmed-temperature gas chromatography and flow control : Linear head pressure programs
title_short Retention in multistep programmed-temperature gas chromatography and flow control : Linear head pressure programs
title_full Retention in multistep programmed-temperature gas chromatography and flow control : Linear head pressure programs
title_fullStr Retention in multistep programmed-temperature gas chromatography and flow control : Linear head pressure programs
title_full_unstemmed Retention in multistep programmed-temperature gas chromatography and flow control : Linear head pressure programs
title_sort retention in multistep programmed-temperature gas chromatography and flow control : linear head pressure programs
publishDate 1997
url http://sedici.unlp.edu.ar/handle/10915/123129
work_keys_str_mv AT gonzalezfranciscor retentioninmultistepprogrammedtemperaturegaschromatographyandflowcontrollinearheadpressureprograms
AT nardilloangelmiguel retentioninmultistepprogrammedtemperaturegaschromatographyandflowcontrollinearheadpressureprograms
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