Mechanical milling of the intermetallic compound AlFe

The intermetallic compound AlFe in its ordered B2 phase has been ground under Ar in a ball-milling device. The system evolution under mechanical work has been examined as a function of time of milling by x-ray diffraction, transmission Mossbauer spectroscopy, and differential scanning calorimetry. S...

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Autores principales: Meyer, Marcos, Mendoza Zélis, Luis Alejandro, Sánchez, Francisco Homero, Clavaguera Mora, M. T., Clavaguera, Narcis
Formato: Articulo
Lenguaje:Inglés
Publicado: 1999
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Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/123103
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id I19-R120-10915-123103
record_format dspace
institution Universidad Nacional de La Plata
institution_str I-19
repository_str R-120
collection SEDICI (UNLP)
language Inglés
topic Ciencias Exactas
Física
Isothermal process
Recrystallization (metallurgy)
Materials science
Diffraction
Intermetallic
Enthalpy
Differential scanning calorimetry
Mössbauer spectroscopy
Activation energy
Thermodynamics
spellingShingle Ciencias Exactas
Física
Isothermal process
Recrystallization (metallurgy)
Materials science
Diffraction
Intermetallic
Enthalpy
Differential scanning calorimetry
Mössbauer spectroscopy
Activation energy
Thermodynamics
Meyer, Marcos
Mendoza Zélis, Luis Alejandro
Sánchez, Francisco Homero
Clavaguera Mora, M. T.
Clavaguera, Narcis
Mechanical milling of the intermetallic compound AlFe
topic_facet Ciencias Exactas
Física
Isothermal process
Recrystallization (metallurgy)
Materials science
Diffraction
Intermetallic
Enthalpy
Differential scanning calorimetry
Mössbauer spectroscopy
Activation energy
Thermodynamics
description The intermetallic compound AlFe in its ordered B2 phase has been ground under Ar in a ball-milling device. The system evolution under mechanical work has been examined as a function of time of milling by x-ray diffraction, transmission Mossbauer spectroscopy, and differential scanning calorimetry. Short and long range disorder was observed. The evolution of the long range order parameter with milling time is analyzed up to the completion of the solid state reaction when a steady state value is reached. The short range order evolution is consistent with a nonstatistical order distribution throughout the sample but mainly distributed in two regions with different degrees of order each. Kinetic analysis of the reordering and recrystallization has been per- formed under continuous heating and isothermal calorimetric regimes. Modeling of these processes is pre- sented as well as the estimated values of both the enthalpy and the activation energy of the reordering process. Results are compared with preceding information on related systems.
format Articulo
Articulo
author Meyer, Marcos
Mendoza Zélis, Luis Alejandro
Sánchez, Francisco Homero
Clavaguera Mora, M. T.
Clavaguera, Narcis
author_facet Meyer, Marcos
Mendoza Zélis, Luis Alejandro
Sánchez, Francisco Homero
Clavaguera Mora, M. T.
Clavaguera, Narcis
author_sort Meyer, Marcos
title Mechanical milling of the intermetallic compound AlFe
title_short Mechanical milling of the intermetallic compound AlFe
title_full Mechanical milling of the intermetallic compound AlFe
title_fullStr Mechanical milling of the intermetallic compound AlFe
title_full_unstemmed Mechanical milling of the intermetallic compound AlFe
title_sort mechanical milling of the intermetallic compound alfe
publishDate 1999
url http://sedici.unlp.edu.ar/handle/10915/123103
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AT sanchezfranciscohomero mechanicalmillingoftheintermetalliccompoundalfe
AT clavagueramoramt mechanicalmillingoftheintermetalliccompoundalfe
AT clavagueranarcis mechanicalmillingoftheintermetalliccompoundalfe
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