A mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing NaHCO<sub>3</sub> and Na<sub>2</sub> CO<sub>3</sub>

The electrochemical behaviour of Cu in solutions containing Na<sub>2</sub>CO<sub>3</sub> + NaHCO<sub>3</sub> (8.8 < pH < 11 .1) has been studied using potentiodynamic and potentiostatic techniques complemented by Scanning Electron Microscopy. The initial sta...

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Autores principales: Pérez Sánchez, M., Souto, R. M., Barrera, M., González, S., Salvarezza, Roberto Carlos, Arvia, Alejandro Jorge
Formato: Articulo
Lenguaje:Inglés
Publicado: 1993
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Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/118514
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id I19-R120-10915-118514
record_format dspace
institution Universidad Nacional de La Plata
institution_str I-19
repository_str R-120
collection SEDICI (UNLP)
language Inglés
topic Ciencias Exactas
Química
Cu corrosion
Cu anodic layers
Nucleation and growth processes
Solution composition
Cu passivation
spellingShingle Ciencias Exactas
Química
Cu corrosion
Cu anodic layers
Nucleation and growth processes
Solution composition
Cu passivation
Pérez Sánchez, M.
Souto, R. M.
Barrera, M.
González, S.
Salvarezza, Roberto Carlos
Arvia, Alejandro Jorge
A mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing NaHCO<sub>3</sub> and Na<sub>2</sub> CO<sub>3</sub>
topic_facet Ciencias Exactas
Química
Cu corrosion
Cu anodic layers
Nucleation and growth processes
Solution composition
Cu passivation
description The electrochemical behaviour of Cu in solutions containing Na<sub>2</sub>CO<sub>3</sub> + NaHCO<sub>3</sub> (8.8 < pH < 11 .1) has been studied using potentiodynamic and potentiostatic techniques complemented by Scanning Electron Microscopy. The initial stages of the anodic layer formation involve the electroformation of a thin inner Cu<sub>2</sub>O layer followed by the growth of a CuO/Cu(OH)<sub>2</sub>-Cu(HO)<sub>3</sub> complex outer layer. Soluble Cu(II) species were detected in the entire anodization potential range . Kinetic models devised for phase change electrochemical processes have been applied to explain the characteristics of anodic and cathodic current transients.
format Articulo
Articulo
author Pérez Sánchez, M.
Souto, R. M.
Barrera, M.
González, S.
Salvarezza, Roberto Carlos
Arvia, Alejandro Jorge
author_facet Pérez Sánchez, M.
Souto, R. M.
Barrera, M.
González, S.
Salvarezza, Roberto Carlos
Arvia, Alejandro Jorge
author_sort Pérez Sánchez, M.
title A mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing NaHCO<sub>3</sub> and Na<sub>2</sub> CO<sub>3</sub>
title_short A mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing NaHCO<sub>3</sub> and Na<sub>2</sub> CO<sub>3</sub>
title_full A mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing NaHCO<sub>3</sub> and Na<sub>2</sub> CO<sub>3</sub>
title_fullStr A mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing NaHCO<sub>3</sub> and Na<sub>2</sub> CO<sub>3</sub>
title_full_unstemmed A mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing NaHCO<sub>3</sub> and Na<sub>2</sub> CO<sub>3</sub>
title_sort mechanistic approach to the electroformation of anodic layers on copper and their electroreduction in aqueous solutions containing nahco<sub>3</sub> and na<sub>2</sub> co<sub>3</sub>
publishDate 1993
url http://sedici.unlp.edu.ar/handle/10915/118514
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