Electrocatalytic hydrogen redox chemistry on gold nanoparticles

Electrocatalytic proton reduction leading to the formation of adsorbed molecular hydrogen on gold nanoparticles of 1-3 and 14-16 nm diameter stabilized by 1-mercapto-undecane-11-tetra(ethyleneglycol) has been demonstrated by cyclic voltammetry using a hanging mercury drop electrode. The nanoparticle...

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Autor principal: Brust, M.
Otros Autores: Gordillo, G.J
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 2012
Acceso en línea:Registro en Scopus
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Registro en la Biblioteca Digital
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024 7 |2 cas  |a ethylene glycol, 107-21-1; hydrogen, 12385-13-6, 1333-74-0 
040 |a Scopus  |b spa  |c AR-BaUEN  |d AR-BaUEN 
030 |a JACSA 
100 1 |a Brust, M. 
245 1 0 |a Electrocatalytic hydrogen redox chemistry on gold nanoparticles 
260 |c 2012 
270 1 0 |m Brust, M.; Department of Chemistry, University of Liverpool, Crown Street, Liverpool L69 7ZD, United Kingdom; email: M.Brust@liv.ac.uk 
506 |2 openaire  |e Política editorial 
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520 3 |a Electrocatalytic proton reduction leading to the formation of adsorbed molecular hydrogen on gold nanoparticles of 1-3 and 14-16 nm diameter stabilized by 1-mercapto-undecane-11-tetra(ethyleneglycol) has been demonstrated by cyclic voltammetry using a hanging mercury drop electrode. The nanoparticles were adsorbed to the electrode from aqueous dispersion and formed robust surface layers transferrable to fresh base electrolyte solutions. Unique electrocatalytic proton redox chemistry was observed that has no comparable counterpart in the electrochemistry of bulk gold electrodes. Depending on size, the nanoparticles have a discrete number of electrocatalytically active sites for the two-electron/two-proton reduction process. The adsorbed hydrogen formed is oxidized with the reverse potential sweep. These findings represent a new example of qualitative different behavior of nanoparticles in comparison with the corresponding bulk material. © 2012 American Chemical Society.  |l eng 
593 |a Department of Chemistry, University of Liverpool, Crown Street, Liverpool L69 7ZD, United Kingdom 
593 |a Departamento de Química Inorgánica, Analítica y Química Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, (1428), Buenos Aires, Argentina 
690 1 0 |a ACTIVE SITE 
690 1 0 |a ADSORBED HYDROGEN 
690 1 0 |a AQUEOUS DISPERSIONS 
690 1 0 |a BASE ELECTROLYTES 
690 1 0 |a BULK MATERIALS 
690 1 0 |a DISCRETE NUMBERS 
690 1 0 |a ELECTROCATALYTIC 
690 1 0 |a GOLD ELECTRODES 
690 1 0 |a GOLD NANOPARTICLES 
690 1 0 |a HANGING MERCURY DROP ELECTRODES 
690 1 0 |a MOLECULAR HYDROGEN 
690 1 0 |a POTENTIAL SWEEP 
690 1 0 |a PROTON REDUCTION 
690 1 0 |a REDOX CHEMISTRY 
690 1 0 |a REDUCTION PROCESS 
690 1 0 |a SURFACE LAYERS 
690 1 0 |a CYCLIC VOLTAMMETRY 
690 1 0 |a ELECTROCATALYSIS 
690 1 0 |a GOLD 
690 1 0 |a HYDROGEN 
690 1 0 |a MERCURY (METAL) 
690 1 0 |a PROTONS 
690 1 0 |a REDUCTION 
690 1 0 |a NANOPARTICLES 
690 1 0 |a 1 MERCAPTO UNDECANE 11 TETRA(ETHYLENEGLYCOL) 
690 1 0 |a ELECTROLYTE 
690 1 0 |a ETHYLENE GLYCOL 
690 1 0 |a GOLD NANOPARTICLE 
690 1 0 |a HYDROGEN 
690 1 0 |a UNCLASSIFIED DRUG 
690 1 0 |a ARTICLE 
690 1 0 |a CATALYST 
690 1 0 |a CYCLIC POTENTIOMETRY 
690 1 0 |a ELECTROCHEMISTRY 
690 1 0 |a ELECTRODE 
690 1 0 |a OXIDATION REDUCTION REACTION 
700 1 |a Gordillo, G.J. 
773 0 |d 2012  |g v. 134  |h pp. 3318-3321  |k n. 7  |p J. Am. Chem. Soc.  |x 00027863  |w (AR-BaUEN)CENRE-19  |t Journal of the American Chemical Society 
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