Mass spectrometry of rhenium complexes: A comparative study by using LDI-MS, MALDI-MS, PESI-MS and ESI-MS
A group of rhenium (I) complexes including in their structure ligands such as CF 3SO 3-, CH 3CO 2-, CO, 2,2′-bipyridine, dipyridil[3,2-a:2′3′-c]phenazine, naphthalene-2-carboxylate, anthracene-9-carboxylate, pyrene-1-carboxylate and 1,10-phenanthroline have been studied for the first time by mass sp...
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2012
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| Acceso en línea: | Registro en Scopus DOI Handle Registro en la Biblioteca Digital |
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| LEADER | 13468caa a22013937a 4500 | ||
|---|---|---|---|
| 001 | PAPER-9799 | ||
| 003 | AR-BaUEN | ||
| 005 | 20230518203946.0 | ||
| 008 | 190411s2012 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-84859021772 | |
| 024 | 7 | |2 cas |a Organometallic Compounds; Rhenium, 7440-15-5 | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 030 | |a JMSPF | ||
| 100 | 1 | |a Petroselli, G. | |
| 245 | 1 | 0 | |a Mass spectrometry of rhenium complexes: A comparative study by using LDI-MS, MALDI-MS, PESI-MS and ESI-MS |
| 260 | |c 2012 | ||
| 270 | 1 | 0 | |m Erra-Balsells, R.; Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Pabellõn II, 3er P., 1428 Buenos Aires, Argentina; email: erra@qo.fcen.uba.ar |
| 506 | |2 openaire |e Política editorial | ||
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| 504 | |a Zhan, Y., Chen, L.C., Suzuki, H., Ariyada, O., Erra-Balsells, R., Nonami, H., Hiraoka, K., Direct profiling of phytochemicals in tulip tissues and in vivo monitoring of the change of carbohydrate content in tulip bulbs by probe electrospray ionization mass spectrometry (2009) J. Am. Soc. Mass Spectrom., 20, p. 2304 | ||
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| 504 | |a Nonami, H., Fukui, S., R Erra-Balsells. β-Carboline alkaloids as matrices for matrix-assisted Ultraviolet Laser Desorption Time-of flight Mass Spectrometry of proteins and sulfated oligosaccharides: A comparative study using phenylcarbonyl compounds, carbazoles and classical matrices (1997) J. Mass Spectrom., 32, p. 287 | ||
| 520 | 3 | |a A group of rhenium (I) complexes including in their structure ligands such as CF 3SO 3-, CH 3CO 2-, CO, 2,2′-bipyridine, dipyridil[3,2-a:2′3′-c]phenazine, naphthalene-2-carboxylate, anthracene-9-carboxylate, pyrene-1-carboxylate and 1,10-phenanthroline have been studied for the first time by mass spectrometry. The probe electrospray ionization (PESI) is a technique based on electrospray ionization (ESI) that generates electrospray from the tip of a solid metal needle. In this work, mass spectra for organometallic complexes obtained by PESI were compared with those obtained by classical ESI and high flow rate electrospray ionization assisted by corona discharge (HF-ESI-CD), an ideal method to avoid decomposition of the complexes and to induce their oxidation to yield intact molecular cation radicals in gas state [M] +. and to produce their reduction yielding the gas species [M] -.. It was found that both techniques showed in general the intact molecular ions of the organometallics studied and provided additional structure characteristic diagnostic fragments. As the rhenium complexes studied in the present work showed strong absorption in the UV-visible region, particularly at 355nm, laser desorption ionization (LDI) mass spectrometry experiments could be conducted. Although intact molecular ions could be detected in a few cases, LDI mass spectra showed diagnostic fragments for characterization of the complexes structure. Furthermore, matrix-assisted laser desorption ionization (MALDI) mass spectra were obtained. Nor-harmane, a compound with basic character, was used as matrix, and the intact molecular ions were detected in two examples, in negative ion mode as the [M] -. species. Results obtained with 2-[(2E)-3-(4-tert-buthylphenyl)-2-methylprop-2-enylidene] malononitrile (DCTB) as matrix are also described. LDI experiments provided more information about the rhenium complex structures than did the MALDI ones. © 2012 John Wiley & Sons, Ltd. |l eng | |
| 593 | |a Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Pabellõn II, 3er P., 1428 Buenos Aires, Argentina | ||
| 593 | |a Clean Energy Research Center, University of Yamanashi Yamanashi, 4-3-11 Takeda, Kofu 400-8511, Japan | ||
| 593 | |a Instituto de Investigaciones Fisicoquímicas Teõricas y Aplicadas (INIFTA, UNLP, CCT la Plata-CONICET), Diag. 113 y 64, B1906ZAA La Plata, Argentina | ||
| 593 | |a Plant Biophysics/Biochemistry Research Laboratory, Faculty of Agriculture, Ehime University, Matsuyama 790-8566, Japan | ||
| 690 | 1 | 0 | |a ACETOXY RHENIUM COMPLEX |
| 690 | 1 | 0 | |a ARYLCARBOXY RHENIUM COMPLEX |
| 690 | 1 | 0 | |a DCTB |
| 690 | 1 | 0 | |a HIGH FLOW RATE ELECTROSPRAY CORONA DISCHARGE |
| 690 | 1 | 0 | |a NOR-HARMANE |
| 690 | 1 | 0 | |a POLYPYRIDIL RHENIUM COMPLEX |
| 690 | 1 | 0 | |a TRIFLUOROMETHANESULFOXY RHENIUM COMPLEX |
| 690 | 1 | 0 | |a ARYLCARBOXY RHENIUM COMPLEX |
| 690 | 1 | 0 | |a DCTB |
| 690 | 1 | 0 | |a HIGH-FLOW RATE |
| 690 | 1 | 0 | |a NOR-HARMANE |
| 690 | 1 | 0 | |a POLYPYRIDIL RHENIUM COMPLEX |
| 690 | 1 | 0 | |a RHENIUM COMPLEXES |
| 690 | 1 | 0 | |a TRIFLUOROMETHANESULFOXY RHENIUM COMPLEX |
| 690 | 1 | 0 | |a CARBON DIOXIDE |
| 690 | 1 | 0 | |a CARBOXYLATION |
| 690 | 1 | 0 | |a ELECTRIC CORONA |
| 690 | 1 | 0 | |a ELECTROSPRAY IONIZATION |
| 690 | 1 | 0 | |a EXPERIMENTS |
| 690 | 1 | 0 | |a FLOW RATE |
| 690 | 1 | 0 | |a ION SOURCES |
| 690 | 1 | 0 | |a IONIZATION OF GASES |
| 690 | 1 | 0 | |a MASS SPECTROMETERS |
| 690 | 1 | 0 | |a MASS SPECTROMETRY |
| 690 | 1 | 0 | |a NAPHTHALENE |
| 690 | 1 | 0 | |a ORGANOMETALLICS |
| 690 | 1 | 0 | |a RHENIUM |
| 690 | 1 | 0 | |a RHENIUM COMPOUNDS |
| 690 | 1 | 0 | |a ORGANOMETALLIC COMPOUND |
| 690 | 1 | 0 | |a RHENIUM COMPLEX |
| 690 | 1 | 0 | |a ARTICLE |
| 690 | 1 | 0 | |a CHEMICAL STRUCTURE |
| 690 | 1 | 0 | |a COMPARATIVE STUDY |
| 690 | 1 | 0 | |a ELECTROSPRAY MASS SPECTROMETRY |
| 690 | 1 | 0 | |a FLOW RATE |
| 690 | 1 | 0 | |a HUMAN |
| 690 | 1 | 0 | |a INTERMETHOD COMPARISON |
| 690 | 1 | 0 | |a MASS SPECTROMETRY |
| 690 | 1 | 0 | |a MATRIX ASSISTED LASER DESORPTION IONIZATION TIME OF FLIGHT MASS SPECTROMETRY |
| 690 | 1 | 0 | |a OXIDATION |
| 690 | 1 | 0 | |a PRIORITY JOURNAL |
| 690 | 1 | 0 | |a PROBE ELECTROSPRAY IONIZATION |
| 690 | 1 | 0 | |a RADIATION ABSORPTION |
| 690 | 1 | 0 | |a ULTRAVIOLET RADIATION |
| 690 | 1 | 0 | |a ORGANOMETALLIC COMPOUNDS |
| 690 | 1 | 0 | |a RHENIUM |
| 690 | 1 | 0 | |a SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION |
| 690 | 1 | 0 | |a SPECTROMETRY, MASS, MATRIX-ASSISTED LASER DESORPTION-IONIZATION |
| 700 | 1 | |a Mandal, M.K. | |
| 700 | 1 | |a Chen, L.C. | |
| 700 | 1 | |a Ruiz, G.T. | |
| 700 | 1 | |a Wolcan, E. | |
| 700 | 1 | |a Hiraoka, K. | |
| 700 | 1 | |a Nonami, H. | |
| 700 | 1 | |a Erra-Balsells, R. | |
| 773 | 0 | |d 2012 |g v. 47 |h pp. 313-321 |k n. 3 |p J. Mass Spectrom. |x 10765174 |t Journal of Mass Spectrometry | |
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| 856 | 4 | 0 | |u https://doi.org/10.1002/jms.2965 |y DOI |
| 856 | 4 | 0 | |u https://hdl.handle.net/20.500.12110/paper_10765174_v47_n3_p313_Petroselli |y Handle |
| 856 | 4 | 0 | |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_10765174_v47_n3_p313_Petroselli |y Registro en la Biblioteca Digital |
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