Spectroscopic, morphological and chemical characterization of historic pigments based on carbon. Paths for the identification of an artistic pigment
Analytical characterization of reference carbon-based black pigments has been performed using Fourier transform infrared spectroscopy (FTIR) with attenuated total reflectance (ATR) and scanning electron microscopy (SEM) coupled to an energy-dispersive X-ray spectrometer (EDS). The unambiguous identi...
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2012
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| Acceso en línea: | Registro en Scopus DOI Handle Registro en la Biblioteca Digital |
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| LEADER | 09928caa a22008297a 4500 | ||
|---|---|---|---|
| 001 | PAPER-9667 | ||
| 003 | AR-BaUEN | ||
| 005 | 20230518203937.0 | ||
| 008 | 190411s2012 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-84856961634 | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 030 | |a MICJA | ||
| 100 | 1 | |a Tomasini, E. | |
| 245 | 1 | 0 | |a Spectroscopic, morphological and chemical characterization of historic pigments based on carbon. Paths for the identification of an artistic pigment |
| 260 | |c 2012 | ||
| 270 | 1 | 0 | |m Maier, M.S.; UMYMFOR and Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, Pabellón 2, (C1428EGA), Ciudad Autónoma de Buenos Aires, Argentina; email: maier@qo.fcen.uba.ar |
| 506 | |2 openaire |e Política editorial | ||
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| 520 | 3 | |a Analytical characterization of reference carbon-based black pigments has been performed using Fourier transform infrared spectroscopy (FTIR) with attenuated total reflectance (ATR) and scanning electron microscopy (SEM) coupled to an energy-dispersive X-ray spectrometer (EDS). The unambiguous identification of these pigments, which are found in paintings, rock art and archeological artifacts, still remains a big challenge due to the variety of sources and manufacturing processes used in their preparation. The analytical results achieved in this study allowed us to discriminate between carbon-based pigments from different sources and detect adulterations. The methodological approach was successfully applied to the identification of vegetable charcoal and bone black in two colonial paintings dated from the eighteenth century. Conclusions regarding the pictorial techniques were drawn from FTIR data. © 2011 Elsevier B.V. |l eng | |
| 536 | |a Detalles de la financiación: Agencia Nacional de Promoción Científica y Tecnológica | ||
| 536 | |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas | ||
| 536 | |a Detalles de la financiación: We thank the following for financial support: Consejo Nacional de Investigaciones Científicas y Técnicas (CONICET) and Agencia Nacional de Promoción Científica y Tecnológica (ANPCyT) ; for painting samples: Carlos Rúa (Centro Nacional de Restauración, La Paz, Bolivia); and for preliminary analysis: Blanca Gómez and Sara D. Parera. E. T. thanks CONICET for a postdoctoral fellowship. M. S. M. and G. S. are Research Members of CONICET. Appendix A | ||
| 593 | |a UMYMFOR and Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, Pabellón 2, (1428) Ciudad Autónoma de Buenos Aires, Argentina | ||
| 593 | |a CONICET, Universidad Nacional de San Martín, B. Quinquela Martín 1784, (1296) Ciudad Autónoma de Buenos Aires, Argentina | ||
| 690 | 1 | 0 | |a ATR |
| 690 | 1 | 0 | |a CARBON BLACK |
| 690 | 1 | 0 | |a CARBON-BASED PIGMENTS |
| 690 | 1 | 0 | |a COLONIAL ART |
| 690 | 1 | 0 | |a FTIR |
| 690 | 1 | 0 | |a SEM-EDS |
| 700 | 1 | |a Siracusano, G. | |
| 700 | 1 | |a Maier, M.S. | |
| 773 | 0 | |d 2012 |g v. 102 |h pp. 28-37 |p Microchem. J. |x 0026265X |w (AR-BaUEN)CENRE-2274 |t Microchemical Journal | |
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