Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum

The cell wall composition of Japanese plums (Prunus salicina) at six developmental stages was previously evaluated (Ponce et al., J. Agric. Food Chem. 2010, 58, 2562-2570). This fruit is an interesting source of pectins, polysaccharides of valuable functionality for pharmaceutical and food formulati...

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Autor principal: Basanta, M.F
Otros Autores: Ponce, N.M.A, Rojas, A.M, Stortz, C.A
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 2012
Acceso en línea:Registro en Scopus
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024 7 |2 cas  |a pectin, 9000-69-5; water, 7732-18-5; pectin; Pectins; Plant Extracts; Water 
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030 |a CAPOD 
100 1 |a Basanta, M.F. 
245 1 0 |a Effect of extraction time and temperature on the characteristics of loosely bound pectins from Japanese plum 
260 |c 2012 
270 1 0 |m Stortz, C.A.; Departamento de Química Orgánica-CIHIDECAR, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, 1428 Buenos Aires, Argentina; email: stortz@qo.fcen.uba.ar 
506 |2 openaire  |e Política editorial 
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520 3 |a The cell wall composition of Japanese plums (Prunus salicina) at six developmental stages was previously evaluated (Ponce et al., J. Agric. Food Chem. 2010, 58, 2562-2570). This fruit is an interesting source of pectins, polysaccharides of valuable functionality for pharmaceutical and food formulations. In the present work it was investigated how the different conditions for the aqueous extraction of pectins from Japanese plums affect the yield as well as their chemical and rheological characteristics. It has been determined that extraction with water at room temperature for periods longer than 2 h did not produce additional increment of yield (12%) but decreased the average molecular weights of the extracted pectins. Pectins with a degree of methylation ≈40% with high viscosity in water and with adequate molecular weights (≈72,000) were obtained. Conversely, utilization of boiling water for extraction increased considerably the yields (33-38%) but the extracted pectins showed significant lower viscosity in water in spite of their higher molecular weights. The poorer thickening ability was associated to the lower proportion of arabinose residues present in the hairy regions of the pectin macromolecules extracted by hot water, which led the polymers to interact more transiently in a 2% w/v water solution. © 2012 Elsevier Ltd. All rights reserved.  |l eng 
536 |a Detalles de la financiación: Universidad de Buenos Aires 
536 |a Detalles de la financiación: Agencia Nacional de Promoción Científica y Tecnológica 
536 |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas 
536 |a Detalles de la financiación: This work was supported by grants from University of Buenos Aires, Agencia Nacional de Promoción Científica y Tecnológica de la República Argentina (ANPCyT) and CONICET . M.F.B. is a recipient of a Fellowship from CONICET, whereas N.M.A.P., A.M.R. and C.A.S. are Research Members of the same Institution. The authors are indebted to Ing. Agr. María D. Raffo for the collection of the plums. 
593 |a Departamento de Química Orgánica-CIHIDECAR, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, 1428 Buenos Aires, Argentina 
593 |a Departamento de Industrias, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, 1428 Buenos Aires, Argentina 
690 1 0 |a FLOW BEHAVIOR 
690 1 0 |a JAPANESE PLUM 
690 1 0 |a PECTINS 
690 1 0 |a VISCOSITY 
690 1 0 |a WATER EXTRACTION 
690 1 0 |a AQUEOUS EXTRACTION 
690 1 0 |a AVERAGE MOLECULAR WEIGHT 
690 1 0 |a BOILING WATER 
690 1 0 |a CELL WALL COMPOSITION 
690 1 0 |a DEGREE OF METHYLATIONS 
690 1 0 |a DEVELOPMENTAL STAGE 
690 1 0 |a EXTRACTION TIME 
690 1 0 |a FLOW BEHAVIORS 
690 1 0 |a HIGH VISCOSITIES 
690 1 0 |a HOT WATER 
690 1 0 |a JAPANESE PLUM 
690 1 0 |a PECTINS 
690 1 0 |a RHEOLOGICAL CHARACTERISTICS 
690 1 0 |a ROOM TEMPERATURE 
690 1 0 |a WATER EXTRACTION 
690 1 0 |a WATER SOLUTIONS 
690 1 0 |a ALKYLATION 
690 1 0 |a MOLECULAR WEIGHT 
690 1 0 |a VISCOSITY 
690 1 0 |a SOLVENT EXTRACTION 
690 1 0 |a PRUNUS 
690 1 0 |a PRUNUS DOMESTICA 
690 1 0 |a PRUNUS SALICINA 
690 1 0 |a PECTIN 
690 1 0 |a PLANT EXTRACT 
690 1 0 |a WATER 
690 1 0 |a CELL WALL 
690 1 0 |a CHEMISTRY 
690 1 0 |a FLOW KINETICS 
690 1 0 |a FRUIT 
690 1 0 |a PRUNUS 
690 1 0 |a SIZE EXCLUSION CHROMATOGRAPHY 
690 1 0 |a TEMPERATURE 
690 1 0 |a TIME 
690 1 0 |a CELL WALL 
690 1 0 |a CHROMATOGRAPHY, GEL 
690 1 0 |a FRUIT 
690 1 0 |a PECTINS 
690 1 0 |a PLANT EXTRACTS 
690 1 0 |a PRUNUS 
690 1 0 |a RHEOLOGY 
690 1 0 |a TEMPERATURE 
690 1 0 |a TIME FACTORS 
690 1 0 |a WATER 
700 1 |a Ponce, N.M.A. 
700 1 |a Rojas, A.M. 
700 1 |a Stortz, C.A. 
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