Crystal structure and spectroscopic properties of polymeric adducts of the tetra-μ-haloaspirinate-dicopper(II)⊥

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Eight new copper(II) complexes with halo-aspirinate anions have been synthesized: [Cu 2(Fasp) 4(MeCN) 2]·2MeCN (1), [Cu 2(Clasp) 4(MeCN) 2]·2MeCN (2), [Cu 2(Brasp) 4 (MeCN) 2]·2MeCN (3), {[Cu 2(Fasp) 4(Pyrz)]·2MeCN} n (4), {[Cu 2(Clasp) 4(Pyrz)]·2MeCN} n (5), [Cu 2(Brasp) 4(Pyrz)] n (6), [Cu 2(Clasp...

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Detalles Bibliográficos
Autor principal: Rustoy, E.M
Otros Autores: Agotegaray, M., Piro, O.E, Castellano, Eduardo Ernesto
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 2012
Acceso en línea:Registro en Scopus
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Biblioteca Central Dr. Luis F. Leloir (FCEN) de Universidad de Buenos Aires
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100 1 |a Rustoy, E.M. 
245 1 0 |a Crystal structure and spectroscopic properties of polymeric adducts of the tetra-μ-haloaspirinate-dicopper(II)⊥ 
260 |c 2012 
270 1 0 |m Rustoy, E.M.; Departamento de Quimica Orgánica y UMYMFOR (CONICET-UBA), Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Pabellón II, 3 Piso, C. Universitaria, Argentina; email: erustoy@qo.fcen.uba.ar 
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506 |2 openaire  |e Política editorial 
520 3 |a Eight new copper(II) complexes with halo-aspirinate anions have been synthesized: [Cu 2(Fasp) 4(MeCN) 2]·2MeCN (1), [Cu 2(Clasp) 4(MeCN) 2]·2MeCN (2), [Cu 2(Brasp) 4 (MeCN) 2]·2MeCN (3), {[Cu 2(Fasp) 4(Pyrz)]·2MeCN} n (4), {[Cu 2(Clasp) 4(Pyrz)]·2MeCN} n (5), [Cu 2(Brasp) 4(Pyrz)] n (6), [Cu 2(Clasp) 4(4,4'-Bipy)] n (7), and [Cu 2(Brasp) 4(4,4'-Bipy)] n (8) (Fasp: fluor-aspirinate; Clasp: chloro-aspirinate; Brasp: bromo-aspirinate; MeCN: acetonitrile; Pyrz: pyrazine; 4,4'-Bipy: 4,4'-bipyridine). The crystal structure of two 2 and 4 have been determined by X-ray diffraction methods. All compounds have been studied employing elemental analysis, IR, and UV-Visible spectroscopic techniques. The results have been compared with previous data reported for complexes with similar structures. © 2012 Taylor & Francis.  |l eng 
536 |a Detalles de la financiación: M24/081 
536 |a Detalles de la financiación: This work was supported in part by the SGCyT of UNS funds (Project M24/081) and by CONICET of Argentina and FAPESP of Brazil. O.E. Piro is a Research Fellow of CONICET. M. Agotegaray is a fellowship holder of CONICET. 
593 |a Departamento de Quimica Orgánica y UMYMFOR (CONICET-UBA), Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Pabellón II, 3 Piso, C. Universitaria, Argentina 
593 |a Departamento de Química, INQUISUR, Universidad Nacional del Sur, Avda. Alem 1253, B8000CPB Bahía Blanca, Argentina 
593 |a Departamento de Física e Instituto IFLP (CONICET, CCT-La Plata), Facultad de Ciencias Exactas, Universidad Nacional de La Plata, C.C. 67, 1900 La Plata, Argentina 
593 |a Instituto de Física de São Paulo, C.P. 369, 13560 São Carlos, SP, Brazil 
690 1 0 |a COPPER(II) COMPLEXES 
690 1 0 |a CRYSTAL STRUCTURES 
690 1 0 |a HALOASPIRINATE ANIONS 
700 1 |a Agotegaray, M. 
700 1 |a Piro, O.E. 
700 1 |a Castellano, Eduardo Ernesto 
773 0 |d 2012  |g v. 65  |h pp. 2341-2352  |k n. 13  |p J. Coord. Chem.  |x 00958972  |w (AR-BaUEN)CENRE-5510  |t Journal of Coordination Chemistry 
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