Vibrational spectra, NMR and theoretical studies of the enantiomers and rotamers of alpha-cypermethrin

NMR, infrared and Raman vibrational spectra of alpha-cypermethrin have been measured at room temperature. Infrared spectra were also recorded to low temperature. The spectra were analyzed by means of ab initio calculations. The conformational space of both enantiomers and some rotamers A, B and C of...

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Autor principal: Jubert, A.H
Otros Autores: Alegre, M.L, Diez, R.P, Pomilio, A.B, Szewczuk, V.D
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 2007
Acceso en línea:Registro en Scopus
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Registro en la Biblioteca Digital
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024 7 |2 cas  |a cipermethrin, 52315-07-8; cypermethrin, 52315-07-8; Pyrethrins 
040 |a Scopus  |b spa  |c AR-BaUEN  |d AR-BaUEN 
030 |a SAMCA 
100 1 |a Jubert, A.H. 
245 1 0 |a Vibrational spectra, NMR and theoretical studies of the enantiomers and rotamers of alpha-cypermethrin 
260 |c 2007 
270 1 0 |m Jubert, A.H.; CEQUINOR, Centro de Química Inorgánica, CONICET, UNLP, CC 962, 1900 La Plata, Argentina; email: jubert@quimica.unlp.edu.ar 
506 |2 openaire  |e Política editorial 
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520 3 |a NMR, infrared and Raman vibrational spectra of alpha-cypermethrin have been measured at room temperature. Infrared spectra were also recorded to low temperature. The spectra were analyzed by means of ab initio calculations. The conformational space of both enantiomers and some rotamers A, B and C of alpha-cypermethrin has been scanned using molecular dynamics and complemented with functional density calculations that optimize the geometry of the lowest-energy conformers of each species as obtained in the simulations. The vibrational frequencies and the 1H and 13C NMR chemical shifts were assigned using functional density calculations. The molecular electrostatic potential maps were obtained and analyzed. © 2006 Elsevier B.V. All rights reserved.  |l eng 
536 |a Detalles de la financiación: Universidad Nacional del Centro de la Provincia de Buenos Aires 
536 |a Detalles de la financiación: National Council for Scientific Research 
536 |a Detalles de la financiación: Universidad Nacional del Centro de la Provincia de Buenos Aires 
536 |a Detalles de la financiación: Centro de Investigación en Computación 
536 |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas 
536 |a Detalles de la financiación: The authors acknowledge CONICET, Universidad Nacional de La Plata and Universidad de Buenos Aires (Argentina) for financial support. A.H.J. is member of the Scientific Research Career (CIC, Provincia de Buenos Aires), Argentina and A.B.P. is senior research member of the National Research Council of Argentina (CONICET, Argentina). 
593 |a CEQUINOR, Centro de Química Inorgánica, CONICET, UNLP, CC 962, 1900 La Plata, Argentina 
593 |a PROPLAME (UBA, CONICET), Departamento de Química Orgánica, Facultad de Ciencias Exactas y Naturales, Pabellon 2, Ciudad Universitaria, C1428EHA Buenos Aires, Argentina 
690 1 0 |a ALPHA-CYPERMETHRIN 
690 1 0 |a DFT 
690 1 0 |a IR 
690 1 0 |a NMR 
690 1 0 |a RAMAN 
690 1 0 |a DENSITY FUNCTIONAL THEORY 
690 1 0 |a ENANTIOMERS 
690 1 0 |a INFRARED SPECTROSCOPY 
690 1 0 |a NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY 
690 1 0 |a RAMAN SCATTERING 
690 1 0 |a VIBRATIONAL SPECTRA 
690 1 0 |a VIBRATIONAL SPECTROSCOPY 
690 1 0 |a ALPHA-CYPERMETHRIN 
690 1 0 |a CONFORMERS 
690 1 0 |a FUNCTIONAL DENSITY CALCULATIONS 
690 1 0 |a ROTAMERS 
690 1 0 |a ORGANIC COMPOUNDS 
690 1 0 |a CIPERMETHRIN 
690 1 0 |a PYRETHROID 
690 1 0 |a ARTICLE 
690 1 0 |a CHEMICAL MODEL 
690 1 0 |a CHEMICAL STRUCTURE 
690 1 0 |a CHEMISTRY 
690 1 0 |a CONFORMATION 
690 1 0 |a ELECTRICITY 
690 1 0 |a INFRARED SPECTROPHOTOMETRY 
690 1 0 |a NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY 
690 1 0 |a RAMAN SPECTROMETRY 
690 1 0 |a STEREOISOMERISM 
690 1 0 |a THERMODYNAMICS 
690 1 0 |a VIBRATION 
690 1 0 |a ELECTROSTATICS 
690 1 0 |a MAGNETIC RESONANCE SPECTROSCOPY 
690 1 0 |a MODELS, CHEMICAL 
690 1 0 |a MODELS, MOLECULAR 
690 1 0 |a MOLECULAR CONFORMATION 
690 1 0 |a PYRETHRINS 
690 1 0 |a SPECTROPHOTOMETRY, INFRARED 
690 1 0 |a SPECTRUM ANALYSIS, RAMAN 
690 1 0 |a STEREOISOMERISM 
690 1 0 |a THERMODYNAMICS 
690 1 0 |a VIBRATION 
700 1 |a Alegre, M.L. 
700 1 |a Diez, R.P. 
700 1 |a Pomilio, A.B. 
700 1 |a Szewczuk, V.D. 
773 0 |d 2007  |g v. 66  |h pp. 1208-1221  |k n. 4-5  |p Spectrochim. Acta Part A Mol. Biomol. Spectrosc.  |x 13861425  |w (AR-BaUEN)CENRE-6900  |t Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy 
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856 4 0 |u https://doi.org/10.1016/j.saa.2006.06.017  |y DOI 
856 4 0 |u https://hdl.handle.net/20.500.12110/paper_13861425_v66_n4-5_p1208_Jubert  |y Handle 
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