Voltammetric and Surface Conductance Study of the Deposition and Stripping of Mercury on Gold

The voltammetric and surface conductance (SC) responses of thin gold film electrodes during the deposition and stripping of mercury in 0.1 M HC104 solutions have been measured for (i) the potential region corresponding to the underpotential deposition (upd) and stripping (ups), (ii) the formation an...

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Autor principal: Romeo, F.M
Otros Autores: Tucceri, R.I, Posadas, D.
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 1990
Acceso en línea:Registro en Scopus
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100 1 |a Romeo, F.M. 
245 1 0 |a Voltammetric and Surface Conductance Study of the Deposition and Stripping of Mercury on Gold 
260 |c 1990 
270 1 0 |m Posadas, D.; Instituto de Investigaciones Fisicoquimicas Tebricas y Aplicadas (INIFTA), Facultad de Ciencias Exactas, Universidad Nacional de La Plata, Sucursal 4, Casilla de Correo 16, 1900 La Plata, Argentina 
506 |2 openaire  |e Política editorial 
504 |a Sherwood, W.G., Bruckenstein, S., (1978) J. Electrochem. Soc., 125, p. 1098 
504 |a Lindstrom, T.R., Johnson, D.C., (1981) Anal. Chem., 53, p. 1855 
504 |a Schadewald, L.A., Lindstrom, T.R., Hussein, W., Evenson, E.E., Johnson, D.C., (1984) J. Electrochem. Soc., 131, p. 1583 
504 |a Shay, M., Bruckenstein, S., (1989) Langmuir, 5 (280) 
504 |a Chauvineau, J.P., Pariset, C., (1973) Surf. Sci., 36 (155) 
504 |a Pariset, C., Chavineau, J.P., (1975) Surf. Sci., 47 (543) 
504 |a Pariset, C., Chavineau, J.P., (1976) Surf. Sci., 57 (363) 
504 |a Pariset, C., Chavineau, J.P., (1978) Surf. Sci., 78 (478) 
504 |a Fujihira, M., Kuwana, T., (1975) Electrochim. Acta, 20 (565) 
504 |a Hansen, W.N., (1980) Surf. Sci., 101 (109) 
504 |a Rath, D.L., (1983) J. Electroanal. Chem., 150 (521) 
504 |a Rath, D.L., (1980) PhD. Thesis, , Utah State University, Utah 
504 |a Ganon, J.P., Clavilier, J., (1984) Surf. Sci., 147 (583) 
504 |a Romeo, F.M., Tucceri, R.I., Posadas, O., (1988) Surf. Sci., 203 (186) 
504 |a Geus, J.W., (1971) Chemisorption and Reactions on Metallic Films, 1, p. 395. , Anderson, J. R., Ed.; Academic Press: London 
504 |a Tucceri, R.I., Posadas, D., (1983) Anal. Asoc. Quim. Arg., 71 (229) 
504 |a Tucceri, R.I., Posadas, D., (1985) J. Electroanal. Chem., 191 (387) 
504 |a Clavilier, J., Faure, R., Guinet, G., Durand, R., (1980) J. Electroanal. Chem., 107 (205) 
504 |a Tucceri, R.I., Posadas, D., (1983) J. Electrochem. Soc., 128, p. 1478 
504 |a Bauer, E., (1984) The Chemical Physics of Solid Surfaces and Heterogeneous Catalysis, 3, p. 20. , King, D. A., Woodruff, D. P., Eds.; Elsevier: Amsterdam 
504 |a Geus, J.W., ref 15, p. 350 
504 |a Faber, T.E., (1972) Introduction to the Theory of Liquid Metals, p. 40. , Cambridge University Press: London 
504 |a Evans, R., Greenwood, D.A., Lloyd, P., Ziman, J.M., (1969) Phys. Lett., 30k (313) 
520 3 |a The voltammetric and surface conductance (SC) responses of thin gold film electrodes during the deposition and stripping of mercury in 0.1 M HC104 solutions have been measured for (i) the potential region corresponding to the underpotential deposition (upd) and stripping (ups), (ii) the formation and stripping of the Hg-Au bulk alloy, and (iii) the deposition and stripping of bulk Hg(0). The analysis of the experimental results shows that the upd mercury grows by an island mechanism up to ὓ 0.7. Linde's surface rule suggests the formation of an interstitial surface phase in this coverage range. The formation of bulk Hg-Au alloy occurs when ὓ = 1 but in the absence of bulk Hg(0). During the stripping of the alloy, the SC is only sensitive to the surface concentration of the Hg(upd) species. Only a relatively small amount of alloy is stripped off during the stripping cycle. It has been verified that the penetration of the mercury atoms into the bulk depends on the grain boundaries concentration. The changes in SC during the formation of bulk Hg(0) indicate that it is a more dense surface phase than the Hg(upd) surface phase. © 1990, American Chemical Society. All rights reserved.  |l eng 
593 |a Departamento de Quimica Fisica, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Pabellon II, Nunez, Buenos Aires, Argentina 
593 |a Instituto de Investigaciones Fisicoquimicas Tebricas y Aplicadas (INIFTA), Facultad de Ciencias Exactas, Universidad Nacional de La Plata, Sucursal 4, Casilla de Correo 16, 1900 La Plata, Argentina 
700 1 |a Tucceri, R.I. 
700 1 |a Posadas, D. 
773 0 |d 1990  |g v. 6  |h pp. 839-842  |k n. 4  |p Langmuir  |x 07437463  |t Langmuir 
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856 4 0 |u https://doi.org/10.1021/la00094a021  |y DOI 
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