Synthesis of [20,21‐13C2]‐progesterone
The synthesis of, [20,21‐13C2]‐progesterone (9) from androst‐4‐ene‐3,17‐dione (1) is described. Labels were introduced by two procedures, namely, condensation of 1 with K13CN and Grignard reaction of nitrile derivative 7 with [13C]‐methylmagnesium iodide. Location of labels was confirmed by 13C‐NMR...
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| Formato: | Capítulo de libro |
| Lenguaje: | Inglés |
| Publicado: |
1991
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| Acceso en línea: | Registro en Scopus DOI Handle Registro en la Biblioteca Digital |
| Aporte de: | Registro referencial: Solicitar el recurso aquí |
| LEADER | 03768caa a22005537a 4500 | ||
|---|---|---|---|
| 001 | PAPER-443 | ||
| 003 | AR-BaUEN | ||
| 005 | 20230518202948.0 | ||
| 008 | 190411s1991 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-0025893692 | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 100 | 1 | |a Caballero, G.M. | |
| 245 | 1 | 0 | |a Synthesis of [20,21‐13C2]‐progesterone |
| 260 | |c 1991 | ||
| 270 | 1 | 0 | |m Caballero, G.M.; Departamento de Quimica Orgánica, Facultad de Ciencias Exactas Y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, Pabellón 2, Buenos Aires, 1428, Argentina |
| 506 | |2 openaire |e Política editorial | ||
| 504 | |a von Wartburg, A., (1964) Helvetica Chimica Acta, 47, p. 1228 | ||
| 504 | |a Porto, A.M., Baralle, F.E., Gros, E.G., (1972) J. Steroid Biochem., 3, p. 11 | ||
| 504 | |a Galagovsky, L.R., Porto, A.M., Burton, G., Maier, M.S., Seldes, A.M., Gros, E.G., (1982) An. Asoc. Quim. Argent., 70, p. 327 | ||
| 504 | |a Galagovsky, L.R., Porto, A.M., Burton, G., Gros, E.G., (1984) Z. Naturforsch., 39 c, p. 38 | ||
| 504 | |a Garraffo, H.M., Gros, E.G., (1982) J. Lab. Compds. Radiopharm., 19, p. 149 | ||
| 504 | |a Porto, A.M., Gros, E.G., Synthesis of PREGN-5-en-3β-o1-20-one-20-14C (1968) Journal of Labelled Compounds, 4, p. 276 | ||
| 504 | |a Nitta, I., Fujimori, S., Ueno, H., (1985) Bull. Chem. Soc. Jpn., 58, p. 978 | ||
| 504 | |a Meyer, K., (1946) Helv. Chim. Acta, 29, p. 1580 | ||
| 504 | |a Hershberg, E.B., Oliveto, E.P., Gerold, C., Johnson, L., (1951) J. Am. Chem. Soc., 73, p. 5073 | ||
| 504 | |a Loewenthal, H.J.E., (1959) Tetrahedron, 6, p. 269 | ||
| 504 | |a Kaye, I.A., Kogon, I.C., (1951) J. Am. Chem. Soc., 73, p. 4893 | ||
| 504 | |a Grieco, P.A., Nishizawa, M., Oguri, T., Burke, S.D., Marinovic, N., (1977) J. Am. Chem. Soc., 99, p. 5773 | ||
| 504 | |a Williams, J.R., Sarkisian, G.M., (1974), p. 32. , ‐ Synthesis; Marker, R.E., (1940) J. Am. Chem. Soc., 62, p. 3350 | ||
| 504 | |a Caballero, G.M., Gros, E.G., (1989), p. 320. , ‐ J. Chem. Res; Bigler, P., (1983) J. Magn. Reson., 55, p. 468 | ||
| 520 | 3 | |a The synthesis of, [20,21‐13C2]‐progesterone (9) from androst‐4‐ene‐3,17‐dione (1) is described. Labels were introduced by two procedures, namely, condensation of 1 with K13CN and Grignard reaction of nitrile derivative 7 with [13C]‐methylmagnesium iodide. Location of labels was confirmed by 13C‐NMR spectroscopy. Copyright © 1991 John Wiley & Sons, Ltd. |l eng | |
| 593 | |a Departamento de Quimica Orgánica, Facultad de Ciencias Exactas Y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, Pabellón 2, Buenos Aires, 1428, Argentina | ||
| 690 | 1 | 0 | |a SYNTHESIS |
| 690 | 1 | 0 | |a [20,21‐13C2]‐PROGESTERONE |
| 690 | 1 | 0 | |a CARBON 13 |
| 690 | 1 | 0 | |a PROGESTERONE |
| 690 | 1 | 0 | |a ARTICLE |
| 690 | 1 | 0 | |a CONTROLLED STUDY |
| 690 | 1 | 0 | |a HORMONE SYNTHESIS |
| 690 | 1 | 0 | |a ISOTOPE LABELING |
| 700 | 1 | |a Gros, E.G. | |
| 773 | 0 | |d 1991 |g v. 29 |h pp. 805-812 |k n. 7 |p J. Label. Compd. Radiopharm. |x 03624803 |w (AR-BaUEN)CENRE-1949 |t Journal of Labelled Compounds and Radiopharmaceuticals | |
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| 856 | 4 | 0 | |u https://doi.org/10.1002/jlcr.2580290711 |y DOI |
| 856 | 4 | 0 | |u https://hdl.handle.net/20.500.12110/paper_03624803_v29_n7_p805_Caballero |y Handle |
| 856 | 4 | 0 | |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_03624803_v29_n7_p805_Caballero |y Registro en la Biblioteca Digital |
| 961 | |a paper_03624803_v29_n7_p805_Caballero |b paper |c PE | ||
| 962 | |a info:eu-repo/semantics/article |a info:ar-repo/semantics/artículo |b info:eu-repo/semantics/publishedVersion | ||
| 999 | |c 61396 | ||