Synthesis and Characterization of some Heterocyclic Derivatives by Cyclization of Carbohydrate Thiosemicarbazones. Part I
We report the synthesis of 2,3-dihydro-1,3,4-thiadiazoles and 1,3,4-thiadiazoles from 1,2:3,4-di-O-isopropylidene-α-D-galacto-1,6-hexodialdo-1,5-pyranose thiosemicarbazone. The physical and spectroscopic characterizations of the heterocyclic derivatives as well as the intermediate product are descri...
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1997
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| 100 | 1 | |a Martins Alho, M.A. | |
| 245 | 1 | 0 | |a Synthesis and Characterization of some Heterocyclic Derivatives by Cyclization of Carbohydrate Thiosemicarbazones. Part I |
| 260 | |c 1997 | ||
| 270 | 1 | 0 | |m Martins Alho, M.A.; Ctro. de Invest. de Hidratos de C., Depto. de Quim. Orgánica, Pabellón II, 3 Piso, C. P. 1428, Buenos Aires, Argentina |
| 506 | |2 openaire |e Política editorial | ||
| 504 | |a Nelson, J.A., Rose, L.M., Bennett, L.L., (1976) J. Cancer Res., 36, p. 1375 | ||
| 504 | |a (1977) Cancer Res., 37, p. 182 | ||
| 504 | |a Miller, W.H., Dessert, A.M., Roblin, R.O., (1950) J. Am. Chem. Soc., 72, p. 4893 | ||
| 504 | |a Gores, E., Hilgetag, Q., Jung, F., (1961) Acta Physiol. Acad. Sci. Hung., 19, p. 95 | ||
| 504 | |a Somogyi, L., (1979) Carbohydr. Res., 75, p. 325 | ||
| 504 | |a El Ashry, E.S., Nassr, M.A., El Kilany, Y., Mousaad, A., (1987) Bull. Chem. Soc. Japan, 60 (9), p. 3405 | ||
| 504 | |a Martins Alho, M.A., D'Accorso, N.B., Thiel, I.M.E., (1996) J. Heterocyclic Chem., 33, p. 1339 | ||
| 504 | |a Lough, C., Hindsgaul, O., Lemieux, R., (1983) Carbohydr. Res., 120, p. 43 | ||
| 504 | |a Bock, K., Pedersen, C., (1983) Adv. Carbohydr. Chem. and Biochem., 41, p. 27 | ||
| 504 | |a El Ashry, E.S., (1983) Carbohydr. Res., 113, p. 273 | ||
| 504 | |a Karabatsos, G.J., Taller, R.A., (1968) Tetrahedron, 24, p. 3347 | ||
| 504 | |a Tronchet, J.M.J., Barbalat-Rey, P., Le-Hong, N., (1971) Helv. Chim. Acta, 54, p. 2615 | ||
| 504 | |a Tronchet, J.M.J., Baehler, B., Jotterand, A., Perret, F., (1971) Helv. Chim. Acta, 54, p. 1660 | ||
| 504 | |a PCMODEL for Windows 5.1 (1994) Serena Software, , MM+ Force Field | ||
| 504 | |a (1995) Hyperchem, , PM3 Force Field | ||
| 504 | |a Tronchet, J.M.J., Neeser, J.R., Charollais, E.J., González, L., (1983) J. Carbohydr. Chem., 2, p. 19 | ||
| 520 | 3 | |a We report the synthesis of 2,3-dihydro-1,3,4-thiadiazoles and 1,3,4-thiadiazoles from 1,2:3,4-di-O-isopropylidene-α-D-galacto-1,6-hexodialdo-1,5-pyranose thiosemicarbazone. The physical and spectroscopic characterizations of the heterocyclic derivatives as well as the intermediate product are described. We present the prefered conformation in solution using computational calculations and spectroscopic data. The possibilities of chiral induction of the cyclization reaction are discussed. |l eng | |
| 593 | |a Ctro. de Invest. de Hidratos de C., Depto. de Quim. Orgánica, Pabellón II, 3 Piso, C. P. 1428, Buenos Aires, Argentina | ||
| 700 | 1 | |a D'Accorso, N.B. | |
| 773 | 0 | |d 1997 |g v. 34 |h pp. 1415-1419 |k n. 5 |p J. Heterocycl. Chem. |x 0022152X |w (AR-BaUEN)CENRE-780 |t Journal of Heterocyclic Chemistry | |
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| 856 | 4 | 0 | |u https://hdl.handle.net/20.500.12110/paper_0022152X_v34_n5_p1415_MartinsAlho |y Handle |
| 856 | 4 | 0 | |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_0022152X_v34_n5_p1415_MartinsAlho |y Registro en la Biblioteca Digital |
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