Mixed-Valent Diruthenium Long-Chain Carboxylates. 2. Magnetic Properties

The magnetic properties of several mixed-valent diruthenium long-chain carboxylates of general formula Ru2(RCO2)4X (X = Cl, DOS, or RCO2, DOS = dodecyl sulfate, and RCO2 = linear aliphatic carboxylate or dialkoxy- or trialkoxybenzoate) were studied in the temperature range 6-400 K. All of the compou...

Descripción completa

Guardado en:
Detalles Bibliográficos
Autor principal: Cukiernik, F.D
Otros Autores: Luneau, D., Marchon, J.-C, Maldivi, P.
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 1998
Acceso en línea:Registro en Scopus
Handle
Registro en la Biblioteca Digital
Aporte de:Registro referencial: Solicitar el recurso aquí
LEADER 08695caa a22008657a 4500
001 PAPER-2902
003 AR-BaUEN
005 20230518203222.0
008 190411s1998 xx ||||fo|||| 00| 0 eng|d
024 7 |2 scopus  |a 2-s2.0-0000347195 
040 |a Scopus  |b spa  |c AR-BaUEN  |d AR-BaUEN 
030 |a INOCA 
100 1 |a Cukiernik, F.D. 
245 1 0 |a Mixed-Valent Diruthenium Long-Chain Carboxylates. 2. Magnetic Properties 
260 |c 1998 
270 1 0 |m Cukiernik, F.D.; Depto. de Quim. Inorgánica, Fac. de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Nuñez (1428) Capital Federal, Argentina 
506 |2 openaire  |e Política editorial 
504 |a Stephenson, T.A., Wilkinson, G.J., (1966) J. Inorg. Nucl. Chem., 8, p. 2285 
504 |a Bennett, M.J., Caulton, K.G., Cotton, F.A., (1969) Inorg. Chem., 8, p. 1 
504 |a Norman, J.G., Renzoni, G.E., Case, D.A., (1979) J. Am. Chem. Soc., 101, p. 5256 
504 |a Cukiernik, F.D., Maldivi, P., Giroud-Godquin, A.M., Marchon, J.C., Ibn-Elhaj, M., Guillon, D., Skoulios, A., (1991) Liq. Cryst., 9, p. 903 
504 |a Cukiernik, F.D., Ibn-Elhaj, M., Chaia, Z.D., Marchon, J.C., Giroud-Godquin, A.M., Guillon, D., Skoulios, A., Maldivi, P., (1998) Chem. Mater., 10, p. 83 
504 |a Mukaida, M., Nomura, T., Ishimori, T., (1972) Bull. Chem. Soc. Jpn., 45, p. 2143 
504 |a Das, B.K., Chakravarty, A.R., (1988) Polyhedron, 7, p. 685 
504 |a Barral, M.C., Jiménez-Aparicio, R., Rial, C., Royer, E., Saucedo, M.J., Urbanos, F.A., (1990) Polyhedron, 9, p. 1723 
504 |a Higgins, P., McCann, M., (1988) J. Chem. Soc., Dalton Trans., p. 661 
504 |a Carvill, A., Higgins, P., McCann, M., Ryan, H., Shiels, A., (1989) J. Chem. Soc., Dalton Trans., p. 2435 
504 |a Telser, J., Drago, R.S., (1984) Inorg. Chem., 23, p. 3114 
504 |a Telser, J., Miskowsky, V.M., Drago, R.S., Wong, N.M., (1985) Inorg. Chem., 24, p. 4765 
504 |a Cukiernik, F.D., Giroud-Godquin, A.M., Maldivi, P., Marchon, J.C., (1994) Inorg. Chim. Acta, 215, p. 203 
504 |a Cotton, F.A., Kim, Y., Ren, T., (1992) Inorg. Chem., 31, p. 2608 
504 |a Cotton, F.A., Kim, Y., Ren, T., (1992) Inorg. Chem., 31, p. 2723 
504 |a note; Cotton, F.A., Kim, Y., Ren, T., (1993) Polyhedron, 12, p. 607 
504 |a Sheldrick, G.M., (1985) Crystallographic Computing, 3, pp. 175-179. , Sheldrick, G. M., Krüger, C, Goddard, R., Eds.; Oxford University Press: England 
504 |a Sheldrick, G.M., (1976) SHELX 76: Program for Crystal Structure Determination, , University of Cambridge: England 
504 |a Cromer, D.T., Waber, J.T., (1974) International Tables for X-ray Crystallography, 4, pp. 99-101. , Ibers, J. A., Hamilton, W. C., Eds.; Kynoch Press: Birmingham, England, Table 2.2B 
504 |a Cromer, D.T., (1974) International Table for X-ray Crystallography, 4, p. 149. , Ibers, J. A., Hamilton. W. C., Eds.; Kynoch Press: Birmingham, England, Table 2.3.1 
504 |a Flack, H.D., (1985) Acta Crystallogr., A41, p. 500 
504 |a Selwood, P.W., (1956) Magnetochemistry, 2nd Ed., p. 78. , Interscience: New York 
504 |a Johnson, C.K., (1965), ORTEP, Report ORNL-3794; Oak Ridge National Laboratory: Oak Ridge, TN; Michalowicz, D.A., Michalowicz, A., MACORTEP; Laboratoire de Physicochimie Structurale, Université Paris Val de Marne, UFR de Sciences et Technologies, 94010 Créteil Marne, UFR de Sciences et Technologies, 94010 Créteil; Lindsay, A.J., Wilkinson, G., Motevalli, M., Hursthouse, M.B., (1987) J. Chem. Soc., Dalton Trans., p. 2723 
504 |a Togano, T., Mukaida, M., Nomura, T., (1980) Bull. Chem. Soc. Jpn., 53, p. 2085 
504 |a Bino, A., Cotton, F.A., Felthouse, T.R., (1979) Inorg. Chem., 18, p. 2599 
504 |a Marsh, R.E., Schomaker, V., (1981) Inorg. Chem., 20, p. 299 
504 |a Kimura, T., Sakurai, T., Shima, M., Togano, T., Mukaida, M., Nomura, T., (1982) Bull Chem. Soc. Jpn., 55, p. 3927 
504 |a Miskowsky, V.M., Loher, T.M., Gray, H.B., (1987) Inorg. Chem., 26, p. 1098 
504 |a McCann, G.M., Canvill, A., Guinan, P., Higgins, P., Campbell, J., Ryan, H., Walsh, M., Gallagher, J., (1991) Polyhedron, 10, p. 2273 
504 |a Das, B.K., Chakravarty, A.R., (1991) Polyhedron, 10, p. 491 
504 |a Barrai, M.C., Jiménez-Aparicio, R., Priego, J.L., Royer, E.C., Gutiérrez-Puebla, E., Ruiz Valero, C., (1992) Polyhedron, 11, p. 2209 
504 |a Martin, D.S., Newman, R.A., Vlasnik, L.S., (1980) Inorg. Chem., 26, p. 3404 
504 |a McCann, M., Carvill, A., Cardin, C., Convery, M., (1993) Polyhedron, 12, p. 1163 
504 |a Cotton, F.A., Matusz, M., Zhong, B., (1988) Inorg. Chem., 27, p. 4368 
504 |a Spohn, M., Strähle, J., Hiller, W., (1986) Z. Natursforsch, 41 B, p. 541 
504 |a O'Connor, C.J., (1982) Prog, Inorg. Chem, 29, p. 203 
504 |a note; note; The simulated powder X-ray diffraction patterns were calculated by E. Amalric (ILL-Grenoble) and J. Laugier (CEA-Grenoble); Hay, P.J., Thibeault, J.C., Hoffmann, R., (1975) J. Am. Chem. Soc., 97, p. 4884 
504 |a Kahn, O., Briat, B., (1976) J. Chem. Soc., Faraday Trans. 2, 72, p. 268 
504 |a Kahn, O., (1984) Magneto-Structural Correlations in Exchange Coupled Systems, p. 37. , Willett, R. D., Gatteschi, D., Kahn, O., Eds.; Nato Asi Series; D. Riedel Publishing Co.: Hingham, MA 
504 |a Estiu, G., Maldivi, P., Cukiemik, F.D., work in progress; Maldivi, P., Giroud-Godquin, A.M., Marchon, J.C., Guillon, D., Skoulios, A., (1989) Chem. Phys. Lett., 157, p. 552 
504 |a Marchon, J.C., Maldivi, P., Giroud-Godquin, A.M., Guillon, D., Skoulios, A., Strommen, D., (1990) Philos. Trans. R. Soc. London, A330, p. 109 
504 |a Bonnet, L., Cukiernik, F.D., Maldivi, P., Giroud-Godquin, A.M., Marchon, J.C., Ibn-Elhaj, M., Guillon, D., Skoulios, A., (1994) Chem. Mater., 6, p. 31 
504 |a Giroud-Godquin, A.M., Latour, J.M., Marchon, J.C., (1985) Inorg. Chem., 24, p. 4452 
504 |a note; Ramos Moita, M.F., Duarte, M.L.T.S., Fausto, R., (1994) J. Chem. Soc., Faraday Trans., 90, p. 2953 
520 3 |a The magnetic properties of several mixed-valent diruthenium long-chain carboxylates of general formula Ru2(RCO2)4X (X = Cl, DOS, or RCO2, DOS = dodecyl sulfate, and RCO2 = linear aliphatic carboxylate or dialkoxy- or trialkoxybenzoate) were studied in the temperature range 6-400 K. All of the compounds exhibit a strong zero-field splitting (D = ca. 75 cm-1), independent of the nature of the axial anion X or of the equatorial substituent R. In the X = RCO2 series an intermolecular antiferromagnetic (AF) interaction zJ = ca. -2 cm-1 was found, whereas in the case of an X = DOS analogue, this interaction is very weak (-0.2 cm-1). The X = Cl series shows three distinct types of interdimer magnetic exchange: very weak, moderate (|zJ| ≈ 2 cm-1), or strong (|zJ| > 10 cm-1). One representative complex in this series, Ru2(C4H9CO2)4Cl, has been structurally characterized by X-ray crystallography. Crystal data: tetragonal system, space group I42d, a = 14.137(3) Å, c = 26.246(5) Å, and Z = 8. Examination of the structures and magnetic behaviors suggests that the AF exchange in this series correlates with the Ru-Cl-Ru intermolecular angle; a qualitative explanation in terms of overlap of magnetic orbitals is proposed. Magnetic susceptibility measurements in the columnar mesophase of the mesomorphic congeners indicate that no significant structural change occurs at the crystal-liquid crystal transition.  |l eng 
593 |a Dept. Rech. Fond. Sur Matiere Cond., Lab. de Chimie de Coordination, CEA-Grenoble, 17 Rue des Martyrs, 38054 Grenoble Cedex 9, France 
593 |a Depto. de Quim. Inorgánica, Fac. de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Nuñez (1428) Capital Federal, Argentina 
700 1 |a Luneau, D. 
700 1 |a Marchon, J.-C. 
700 1 |a Maldivi, P. 
773 0 |d 1998  |g v. 37  |h pp. 3698-3704  |k n. 15  |p Inorg. Chem.  |x 00201669  |w (AR-BaUEN)CENRE-60  |t Inorganic Chemistry 
856 4 1 |u https://www.scopus.com/inward/record.uri?eid=2-s2.0-0000347195&partnerID=40&md5=d99d8561dd5801b390c6fa9991c4a121  |y Registro en Scopus 
856 4 0 |u https://hdl.handle.net/20.500.12110/paper_00201669_v37_n15_p3698_Cukiernik  |y Handle 
856 4 0 |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_00201669_v37_n15_p3698_Cukiernik  |y Registro en la Biblioteca Digital 
961 |a paper_00201669_v37_n15_p3698_Cukiernik  |b paper  |c PE 
962 |a info:eu-repo/semantics/article  |a info:ar-repo/semantics/artículo  |b info:eu-repo/semantics/publishedVersion 
963 |a VARI 
999 |c 63855