Hierarchically structured TiO 2 -based composites for Fenton-type oxidation processes

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A novel hierarchically structured composite aimed as a stable catalyst for the heterogeneous Fenton-type (HFT) oxidation process was developed by using a cost-effective and versatile technique. Prussian Blue nanoparticles (PBNP) were dispersed onto aligned macroporous TiO 2 (rutile) monoliths prepar...

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Autor principal: Doumic, L.I
Otros Autores: Génova, M., Žerjav, G., Pintar, A., Cassanello, M.C, Romeo, H.E, Ayude, M.A
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: Academic Press 2019
Acceso en línea:Registro en Scopus
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024 7 |2 cas  |a ferrous gluconate, 299-29-6; hydrogen peroxide, 7722-84-1; hydroxyl radical, 3352-57-6; titanium dioxide, 1317-70-0, 1317-80-2, 13463-67-7, 51745-87-0 
040 |a Scopus  |b spa  |c AR-BaUEN  |d AR-BaUEN 
030 |a JEVMA 
100 1 |a Doumic, L.I. 
245 1 0 |a Hierarchically structured TiO 2 -based composites for Fenton-type oxidation processes 
260 |b Academic Press  |c 2019 
270 1 0 |m Doumic, L.I.; Catalizadores y Superficies, INTEMA, Facultad de Ingeniería, UNMdP, Av. Juan.B. Justo 4302, Argentina; email: luciladoumic@fi.mdp.edu.ar 
506 |2 openaire  |e Política editorial 
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520 3 |a A novel hierarchically structured composite aimed as a stable catalyst for the heterogeneous Fenton-type (HFT) oxidation process was developed by using a cost-effective and versatile technique. Prussian Blue nanoparticles (PBNP) were dispersed onto aligned macroporous TiO 2 (rutile) monoliths prepared via directional freezing of aqueous dispersions of TiO 2 nanoparticles. The catalytic performance was evaluated in the HFT oxidation of an azo dye frequently used as a model contaminant, Orange G (OG). Experiments were carried out in a liquid batch-recycle reactor, in which the liquid flow rate was set to ensure negligible external mass transfer resistance. The catalyst exhibited good activity to form highly oxidative radicals from hydrogen peroxide decomposition, which readily discolored OG. Significant reduction of the time required to attain complete discoloration and improvement in TOC removal were achieved by adjusting operating conditions and oxidant dosage strategies. Almost complete OG conversion at around 90 min and 34.4% of TOC removal after 4 h were achieved by using the best evaluated strategy. The catalyst activity was tested under specific operating conditions and remained unaltered during 42 cycles of 4 h each (total 168 h). The fresh and used PBNP/TiO 2 catalysts and the support were thoroughly characterized by several techniques. Results supported the excellent stability exhibited by the catalyst in the OG HFT oxidation. © 2019 Elsevier Ltd  |l eng 
536 |a Detalles de la financiación: Center for Outcomes Research and Evaluation, Yale School of Medicine, CORE 
536 |a Detalles de la financiación: Universidad de Buenos Aires, UBA 
536 |a Detalles de la financiación: Javna Agencija za Raziskovalno Dejavnost RS, ARRS 
536 |a Detalles de la financiación: Ministry of Science, Technology and Space 
536 |a Detalles de la financiación: Ministerio de Ciencia, Tecnología e Innovación Productiva, MINCyT, PICT2016-0083 
536 |a Detalles de la financiación: Agencia Nacional de Promoción Científica y Tecnológica, ANPCyT 
536 |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas, CONICET 
536 |a Detalles de la financiación: Financial support from CONICET, Argentina ; UBA, Argentina ; UNMdP, Argentina ; ANPCyT, Argentina ; Cooperation program between the Ministry of Science, Technology and Productive Innovation, Argentina and the Ministry of Higher Education, Science and Technology, Slovenia (MINCYT - MHEST) and ANPCyT ( PICT2016-0083 ). is gratefully acknowledged. G. Žerjav and A. Pintar acknowledge the financial support from the Slovenian Research Agency (research core funding No. P2-0150 ). We express our gratitude to Dr. Rodrigo Parra, Tech. P. Kalafatovich and Tech. H. Asencio for their valuable support. Appendix A 
593 |a División Catalizadores y Superficies, INTEMA-CONICET, Departamento de Ingeniería Química, Facultad de Ingeniería, UNMdP, Av. Juan B. Justo 4302, Mar del Plata, B7608FDQ, Argentina 
593 |a Department for Environmental Sciences and Engineering, National Institute of Chemistry, Hajdrihova 19, Ljubljana, SI-1001, Slovenia 
593 |a LARSI, Dep. Industrias, FCEyN, Universidad de Buenos Aires, Int. Güiraldes 2620, Buenos Aires, C1428BGA, Argentina 
593 |a División Polímeros Nanoestructurados, INTEMA-CONICET, Facultad de Ingeniería, UNMdP, Av. Juan B. Justo 4302, Mar del Plata, B7608FDQ, Argentina 
690 1 0 |a HETEROGENEOUS FENTON-TYPE OXIDATION 
690 1 0 |a HIERARCHICALLY STRUCTURED POROUS MATERIALS 
690 1 0 |a PRUSSIAN BLUE NANOPARTICLES 
690 1 0 |a STABILITY 
690 1 0 |a FERROUS GLUCONATE 
690 1 0 |a HYDROGEN PEROXIDE 
690 1 0 |a HYDROXYL RADICAL 
690 1 0 |a ORGANIC COMPOUND 
690 1 0 |a OXIDIZING AGENT 
690 1 0 |a TITANIUM DIOXIDE 
690 1 0 |a CATALYSIS 
690 1 0 |a CATALYST 
690 1 0 |a COMPOSITE 
690 1 0 |a DISPERSION 
690 1 0 |a DYE 
690 1 0 |a EXPERIMENT 
690 1 0 |a HYDROGEN PEROXIDE 
690 1 0 |a MASS TRANSFER 
690 1 0 |a NANOPARTICLE 
690 1 0 |a OXIDATION 
690 1 0 |a OXIDE 
690 1 0 |a POROUS MEDIUM 
690 1 0 |a RUTILE 
690 1 0 |a TITANIUM 
690 1 0 |a TOTAL ORGANIC CARBON 
690 1 0 |a ADSORPTION 
690 1 0 |a ARTICLE 
690 1 0 |a CATALYST 
690 1 0 |a DECOMPOSITION 
690 1 0 |a FENTON REACTION 
690 1 0 |a FIELD EMISSION SCANNING ELECTRON MICROSCOPY 
690 1 0 |a FLOW RATE 
690 1 0 |a FOURIER TRANSFORM INFRARED SPECTROSCOPY 
690 1 0 |a HEAT TREATMENT 
690 1 0 |a HYSTERESIS 
690 1 0 |a LIQUID 
690 1 0 |a MINERALIZATION 
690 1 0 |a OXIDATION 
690 1 0 |a POROSITY 
690 1 0 |a SURFACE AREA 
690 1 0 |a TEMPERATURE 
690 1 0 |a THERMOGRAVIMETRY 
690 1 0 |a X RAY DIFFRACTION 
700 1 |a Génova, M. 
700 1 |a Žerjav, G. 
700 1 |a Pintar, A. 
700 1 |a Cassanello, M.C. 
700 1 |a Romeo, H.E. 
700 1 |a Ayude, M.A. 
773 0 |d Academic Press, 2019  |g v. 236  |h pp. 591-602  |p J. Environ. Manage.  |x 03014797  |w (AR-BaUEN)CENRE-754  |t Journal of Environmental Management 
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