Natural attenuation of oil spills in Patagonian soils. Characterization by 1H NMR spectroscopy
The natural attenuation of oil spill contaminated soils, with different exposure times, in Patagonian environment was evaluated by the use of several parameters to quantify the degree of changes in the composition. Column (CC) and gas chromatography (GC); UV-visible and 1H NMR techniques were used t...
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2008
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| LEADER | 13291caa a22014657a 4500 | ||
|---|---|---|---|
| 001 | PAPER-22487 | ||
| 003 | AR-BaUEN | ||
| 005 | 20230518205403.0 | ||
| 008 | 190411s2008 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-41649089012 | |
| 024 | 7 | |2 cas |a petroleum, 8002-05-9; Fertilizers; Petroleum; Soil; Soil Pollutants | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 030 | |a ENVTE | ||
| 100 | 1 | |a Ríos, S.M. | |
| 245 | 1 | 0 | |a Natural attenuation of oil spills in Patagonian soils. Characterization by 1H NMR spectroscopy |
| 260 | |c 2008 | ||
| 270 | 1 | 0 | |m Nudelman, N. S.; Department of Organic Chemistry, Universidad de Buenos Aires, Ciudad Universitaria, 1428 Buenos Aires, Argentina |
| 506 | |2 openaire |e Política editorial | ||
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| 520 | 3 | |a The natural attenuation of oil spill contaminated soils, with different exposure times, in Patagonian environment was evaluated by the use of several parameters to quantify the degree of changes in the composition. Column (CC) and gas chromatography (GC); UV-visible and 1H NMR techniques were used to determine compositional and structural indexes. The results show that the nC18/Phytane GC index, that was 1.5 for crude oil, decreased with exposure time to values between 0.97-0.17 in the residues. The percentages for the four aliphatic (H1 - H4) and the aromatic (HA) proton types, determined by 1H NMR, were: 12.9-34.4 (H1), 43.3-60.2 (H2), 4.24-24.2 (H3), 1.33-17.9 (H4), and 0.44-4.81 (HA), in crude oil and residues, respectively. Furthermore, the characterization of significant 1H NMR signals indicated the presence of carboxylic acid hydrogens in the polar fraction of the crude oil and of residues of two years age. The Principal Components Analysis (PCA) of the parameters determined by CC, GC and NMR showed that the first three principal components (1st, 2nd, and 3rd PC), accounted for more than 84% of variance. The 1st PC is largely influenced by H3, H1, H4, H2, and the nC18/Phytane GC parameter, in the order given. The evaluation of the different parameters by PCA suggests that 1H NMR is more useful than GC to evaluate the degree of the chemical transformations of oil spills in soils. © Taylor & Francis, 2008. |l eng | |
| 536 | |a Detalles de la financiación: Universidad de Buenos Aires | ||
| 536 | |a Detalles de la financiación: National Research Council | ||
| 536 | |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas | ||
| 536 | |a Detalles de la financiación: Thanks are given to O. Katusich (UNPSJB) for technical assistance, and to M. Mas (UNPSJB) for help in the statistics calculations. Financial support from the University of Buenos Aires; the University of La Patagonia San Juan Bosco (UNPSJB) and from the National Research Council from Argentina (CONICET) is gratefully acknowledged. | ||
| 593 | |a Department of Chemistry, Universidad Nacional de la Patagonia San Juan Bosco, Ciudad Universitaria, km4, Comodoro Rivadavia, (9004) Chubut, Argentina | ||
| 593 | |a Department of Organic Chemistry, Universidad de Buenos Aires, Ciudad Universitaria, 1428 Buenos Aires, Argentina | ||
| 690 | 1 | 0 | |a COMPOSITIONAL PARAMETERS |
| 690 | 1 | 0 | |a ENVIRONMENTAL EXPOSURE |
| 690 | 1 | 0 | |a NMR SPECTRA OF PETROLEUM SAMPLES |
| 690 | 1 | 0 | |a OIL SPILL BEHAVIOR |
| 690 | 1 | 0 | |a PATAGONIAN SOILS |
| 690 | 1 | 0 | |a PETROLEUM RESIDUES |
| 690 | 1 | 0 | |a ALIPHATIC COMPOUND |
| 690 | 1 | 0 | |a AROMATIC COMPOUND |
| 690 | 1 | 0 | |a CARBOXYLIC ACID |
| 690 | 1 | 0 | |a HYDROCARBON |
| 690 | 1 | 0 | |a PETROLEUM |
| 690 | 1 | 0 | |a GAS CHROMATOGRAPHY |
| 690 | 1 | 0 | |a NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY |
| 690 | 1 | 0 | |a OIL SPILLS |
| 690 | 1 | 0 | |a PARAMETER ESTIMATION |
| 690 | 1 | 0 | |a SOIL SURVEYS |
| 690 | 1 | 0 | |a CARBOXYLIC ACID |
| 690 | 1 | 0 | |a CRUDE OIL |
| 690 | 1 | 0 | |a GAS CHROMATOGRAPHY |
| 690 | 1 | 0 | |a NATURAL ATTENUATION |
| 690 | 1 | 0 | |a NUCLEAR MAGNETIC RESONANCE |
| 690 | 1 | 0 | |a OIL SPILL |
| 690 | 1 | 0 | |a PRINCIPAL COMPONENT ANALYSIS |
| 690 | 1 | 0 | |a SOIL POLLUTION |
| 690 | 1 | 0 | |a TRANSFORMATION |
| 690 | 1 | 0 | |a ANALYSIS OF VARIANCE |
| 690 | 1 | 0 | |a ARTICLE |
| 690 | 1 | 0 | |a CHEMICAL ANALYSIS |
| 690 | 1 | 0 | |a CHEMICAL COMPOSITION |
| 690 | 1 | 0 | |a COLUMN CHROMATOGRAPHY |
| 690 | 1 | 0 | |a ENVIRONMENTAL IMPACT |
| 690 | 1 | 0 | |a EXPOSURE |
| 690 | 1 | 0 | |a GAS CHROMATOGRAPHY |
| 690 | 1 | 0 | |a OIL SPILL |
| 690 | 1 | 0 | |a PARAMETER |
| 690 | 1 | 0 | |a PRINCIPAL COMPONENT ANALYSIS |
| 690 | 1 | 0 | |a PROTON NUCLEAR MAGNETIC RESONANCE |
| 690 | 1 | 0 | |a PROTON TRANSPORT |
| 690 | 1 | 0 | |a QUANTITATIVE ANALYSIS |
| 690 | 1 | 0 | |a SOIL ANALYSIS |
| 690 | 1 | 0 | |a SOIL POLLUTION |
| 690 | 1 | 0 | |a ULTRAVIOLET RADIATION |
| 690 | 1 | 0 | |a BIODEGRADATION, ENVIRONMENTAL |
| 690 | 1 | 0 | |a CHROMATOGRAPHY, GAS |
| 690 | 1 | 0 | |a FERTILIZERS |
| 690 | 1 | 0 | |a MAGNETIC RESONANCE SPECTROSCOPY |
| 690 | 1 | 0 | |a PETROLEUM |
| 690 | 1 | 0 | |a PRINCIPAL COMPONENT ANALYSIS |
| 690 | 1 | 0 | |a SOIL |
| 690 | 1 | 0 | |a SOIL POLLUTANTS |
| 690 | 1 | 0 | |a PATAGONIA |
| 651 | 4 | |a ARGENTINA | |
| 651 | 4 | |a SOUTH AMERICA | |
| 700 | 1 | |a Nudelman, N.S. | |
| 773 | 0 | |d 2008 |g v. 29 |h pp. 23-33 |k n. 1 |p Environ. Technol. |x 09593330 |t Environmental Technology | |
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| 856 | 4 | 0 | |u https://doi.org/10.1080/09593330802008446 |y DOI |
| 856 | 4 | 0 | |u https://hdl.handle.net/20.500.12110/paper_09593330_v29_n1_p23_Rios |y Handle |
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