Solid state coordination chemistry of pyridinedicarboxylic acid isomers. III Synthesis and crystal structures of complexes of Zn and Ni with lutidinic acid (lutidinic = 2,4-pyridinedicarboxylic)
The synthesis and the crystal and molecular structures of three metal(II) derivatives of lutidinic acid are presented (lutidinic acid = 2,4-pyridinedicarboxylic acid = H22,4-pydc). Zn(2,4-pydc)(H2O)4]·H2O crystallizes in the monoclinic space group P21/c, with a = 7.764(3), b = 6.546(3), c = 22.021(8...
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| Otros Autores: | , , , |
| Formato: | Capítulo de libro |
| Lenguaje: | Inglés |
| Publicado: |
2003
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| Acceso en línea: | Registro en Scopus DOI Handle Registro en la Biblioteca Digital |
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| LEADER | 06324caa a22008657a 4500 | ||
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| 001 | PAPER-21671 | ||
| 003 | AR-BaUEN | ||
| 005 | 20241206083244.0 | ||
| 008 | 190411s2003 xx ||||fo|||| 00| 0 eng|d | ||
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| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 100 | 1 | |a Sileo, E.E. | |
| 245 | 1 | 0 | |a Solid state coordination chemistry of pyridinedicarboxylic acid isomers. III Synthesis and crystal structures of complexes of Zn and Ni with lutidinic acid (lutidinic = 2,4-pyridinedicarboxylic) |
| 260 | |c 2003 | ||
| 270 | 1 | 0 | |m Sileo, E.E.; Departamento de Quimica Inorganica, Facultad de Ciencias Exactas y Nat., Universidad de Buenos Aires, Pab. II, 1428EHA Buenos Aires, Argentina; email: sileo@qi.fcen.uba.ar |
| 504 | |a Sileo, E.E., Rigotti, G., Rivero, B.E., Blesa, M.A., (1997) J. Phys. Chem. Solids, 58, p. 1127 | ||
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| 504 | |a Sileo, E.E., Vega, D., Baggio, R., Garland, M.T., Blesa, M.A., (1999) Aust. J. Chem., 52, p. 205 | ||
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| 504 | |a Sheldrick, G.M., (1990) Acta Crystallogr., A46, p. 467 | ||
| 504 | |a Sheldrick, G.M., (1993) SHELXL93. A Program for Crystal Structure Refinement, , University of Gottingen, Germany | ||
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| 506 | |2 openaire |e Política editorial | ||
| 520 | 3 | |a The synthesis and the crystal and molecular structures of three metal(II) derivatives of lutidinic acid are presented (lutidinic acid = 2,4-pyridinedicarboxylic acid = H22,4-pydc). Zn(2,4-pydc)(H2O)4]·H2O crystallizes in the monoclinic space group P21/c, with a = 7.764(3), b = 6.546(3), c = 22.021(8) Å, β = 91.45(4)°; and Z = 4. Na2[Zn(2,4-pydc)2(H2- O)2]·8H2O crystallizes in P21/a, with a = 7.070(2), b = 13.630(2), c = 12.520(1) Å; β = 91.66(1)°; and Z = 2. [Ni(H2O)6][Ni(2,4-pydc)2 (H2O)2] crystallizes in the triclinic space group P - 1, with a = 5.200(7), b = 7.890(3), c = 13.872(5) Å; a = 84.96(3), β = 85.64(2)°, γ = 73.21(4); and Z = 2. The Zn and Ni ions are hexacoordinated and the lutidinate group is almost planar binding the metal through an oxygen atom from the 2-carboxylate group. All compounds present a dangling uncoordinated 4-carboxylate group. The stereochemistry of the title compounds is compared with other metal (II) pyridinedicarboxylates. © 2002 Elsevier Science B.V. All rights reserved. |l eng | |
| 536 | |a Detalles de la financiación: Pict 06-06631 | ||
| 536 | |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas | ||
| 536 | |a Detalles de la financiación: This work was supported by CONICET, CICPBA and ANPCyT Pict 06-06631 of Argentina and by FAPESP and VITAE Foundation of Brazil. Part of the X-ray diffraction experiments were carried out at the National Diffraction Laboratory (LANADI), La Plata, Argentina. G.E. Rigotti is a member of the Comisión de Investigaciones Cientı́ficas, Provincia de Buenos Aires. | ||
| 593 | |a Departamento de Quimica Inorganica, Facultad de Ciencias Exactas y Nat., Universidad de Buenos Aires, Pab. II, 1428EHA Buenos Aires, Argentina | ||
| 593 | |a Instituto de Fisica de Sao Carlos, Universidade de São Paulo, C.P. 369, 13560 Sao Carlos (SP), Brazil | ||
| 593 | |a Departamento de Física, Facultad de Ciencias Exactas, Universidad Nacional de La Plata, C.C. 67, 1900 La Plata, Argentina | ||
| 690 | 1 | 0 | |a 2,4-PYRIDINEDICARBOXYLATE |
| 690 | 1 | 0 | |a CRYSTAL STRUCTURE |
| 690 | 1 | 0 | |a LUTIDINATE |
| 690 | 1 | 0 | |a NICKEL |
| 690 | 1 | 0 | |a ZINC |
| 690 | 1 | 0 | |a 2,4 PYRIDINEDICARBOXYLIC ACID |
| 690 | 1 | 0 | |a COORDINATION COMPOUND |
| 690 | 1 | 0 | |a NICKEL COMPLEX |
| 690 | 1 | 0 | |a OXYGEN |
| 690 | 1 | 0 | |a PYRIDINEDICARBOXYLIC ACID |
| 690 | 1 | 0 | |a UNCLASSIFIED DRUG |
| 690 | 1 | 0 | |a ZINC COMPLEX |
| 690 | 1 | 0 | |a ARTICLE |
| 690 | 1 | 0 | |a CHEMICAL BINDING |
| 690 | 1 | 0 | |a CRYSTAL STRUCTURE |
| 690 | 1 | 0 | |a CRYSTALLIZATION |
| 690 | 1 | 0 | |a ISOMER |
| 690 | 1 | 0 | |a STEREOCHEMISTRY |
| 690 | 1 | 0 | |a STRUCTURE ANALYSIS |
| 700 | 1 | |a De Araujo, A.S. | |
| 700 | 1 | |a Rigotti, G. | |
| 700 | 1 | |a Piro, O.E. | |
| 700 | 1 | |a Castellano, Eduardo Ernesto | |
| 773 | 0 | |d 2003 |g v. 644 |h pp. 67-76 |k n. 1-3 |p J. Mol. Struct. |x 00222860 |w (AR-BaUEN)CENRE-222 |t Journal of Molecular Structure | |
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