Synthesis and characterization of some heterocyclic derivatives by cyclization of carbohydrate thiosemicarbazone - Part III
Synthesis of (3′R) 2-acetamido-4-N-acetyl-3′-spiro-[1′,2′:5′,6′- di-O-isopropylidene-α-D-glucofuranosyl]1,3,4-thiadiazoline diastereomerically pure is described. We report the physical and spectroscopic characterization of the new heterocyclic compound as well as its immediate precursors. We discuss...
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| Formato: | Capítulo de libro |
| Lenguaje: | Inglés |
| Publicado: |
2002
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| Acceso en línea: | Registro en Scopus Handle Registro en la Biblioteca Digital |
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| LEADER | 03554caa a22006017a 4500 | ||
|---|---|---|---|
| 001 | PAPER-20439 | ||
| 003 | AR-BaUEN | ||
| 005 | 20230518205150.0 | ||
| 008 | 190411s2002 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-0036191367 | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 030 | |a JHTCA | ||
| 100 | 1 | |a Martins Alho, M.A. | |
| 245 | 1 | 0 | |a Synthesis and characterization of some heterocyclic derivatives by cyclization of carbohydrate thiosemicarbazone - Part III |
| 260 | |c 2002 | ||
| 270 | 1 | 0 | |m Martins Alho, M.A.; Fac. de Ciencias Exactas/Naturales, Universidad de Buenos Aires, Ciudad Universitaria, C. P. 1428, Buenos Aires, Argentina |
| 506 | |2 openaire |e Política editorial | ||
| 504 | |a Martins Alho, M.A., D'Accorso, N.B., (1997) J. Heterocyclic Chem., 34, p. 1415 | ||
| 504 | |a Martins Alho, M.A., D'Accorso, N.B., (2000) J. Heterocyclic Chem., 37, p. 811 | ||
| 504 | |a Onodera, K., Kashimura, N., (1972) Methods in Carbohydrate Chemistry, 6, p. 334. , R. L. Whistler and J. N. BeMiller, ed, Academic Press, New York and London | ||
| 504 | |a Karabatsos, G.J., Taller, R.A., (1968) Tetrahedron, 24, p. 3347 | ||
| 504 | |a Tronchet, J.M.J., Gentile, B., (1976) Helvetica Chim. Acta., 54, p. 1380 | ||
| 504 | |a Rosenthal, A., Ong, K.S., Baker, D., (1970) Carbohydr. Res., 13, p. 113 | ||
| 504 | |a Tronchet, J.M.J., Neeser, J.R., Charollais, E.J., González, L., (1983) J. Carbohydrate Chem., 2, p. 19 | ||
| 504 | |a Martins Alho, M.A., D'Accorso, N.B., (2000) Carbohydr. Res., 328, p. 481 | ||
| 520 | 3 | |a Synthesis of (3′R) 2-acetamido-4-N-acetyl-3′-spiro-[1′,2′:5′,6′- di-O-isopropylidene-α-D-glucofuranosyl]1,3,4-thiadiazoline diastereomerically pure is described. We report the physical and spectroscopic characterization of the new heterocyclic compound as well as its immediate precursors. We discuss also the possibilities for cyclization and established the stereochemistry of the new stereogenic center. |l eng | |
| 593 | |a Fac. de Ciencias Exactas/Naturales, Universidad de Buenos Aires, Ciudad Universitaria, C. P. 1428, Buenos Aires, Argentina | ||
| 690 | 1 | 0 | |a 2 ACETAMIDO 4 N ACETYL 3' SPIRO[1',2':5',6' DI O ISOPROPYLIDENE ALPHA DEXTRO GLUCOFURANOSYL] 1,3,4 THIADIAZOLINE |
| 690 | 1 | 0 | |a CARBOHYDRATE |
| 690 | 1 | 0 | |a HETEROCYCLIC COMPOUND |
| 690 | 1 | 0 | |a THIOSEMICARBAZONE DERIVATIVE |
| 690 | 1 | 0 | |a UNCLASSIFIED DRUG |
| 690 | 1 | 0 | |a ARTICLE |
| 690 | 1 | 0 | |a CARBON NUCLEAR MAGNETIC RESONANCE |
| 690 | 1 | 0 | |a CHEMICAL STRUCTURE |
| 690 | 1 | 0 | |a CHIRALITY |
| 690 | 1 | 0 | |a CYCLIZATION |
| 690 | 1 | 0 | |a DIASTEREOISOMER |
| 690 | 1 | 0 | |a ISOMERISM |
| 690 | 1 | 0 | |a NUCLEAR OVERHAUSER EFFECT |
| 690 | 1 | 0 | |a PROTON NUCLEAR MAGNETIC RESONANCE |
| 690 | 1 | 0 | |a SPECTROSCOPY |
| 690 | 1 | 0 | |a STEREOCHEMISTRY |
| 690 | 1 | 0 | |a SYNTHESIS |
| 700 | 1 | |a D' Accorso, N.B. | |
| 773 | 0 | |d 2002 |g v. 39 |h pp. 137-140 |k n. 1 |p J. Heterocycl. Chem. |x 0022152X |w (AR-BaUEN)CENRE-780 |t Journal of Heterocyclic Chemistry | |
| 856 | 4 | 1 | |u https://www.scopus.com/inward/record.uri?eid=2-s2.0-0036191367&partnerID=40&md5=4aeb47697562629921d3a84b5187214d |y Registro en Scopus |
| 856 | 4 | 0 | |u https://hdl.handle.net/20.500.12110/paper_0022152X_v39_n1_p137_MartinsAlho |y Handle |
| 856 | 4 | 0 | |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_0022152X_v39_n1_p137_MartinsAlho |y Registro en la Biblioteca Digital |
| 961 | |a paper_0022152X_v39_n1_p137_MartinsAlho |b paper |c PE | ||
| 962 | |a info:eu-repo/semantics/article |a info:ar-repo/semantics/artículo |b info:eu-repo/semantics/publishedVersion | ||
| 963 | |a VARI | ||
| 999 | |c 81392 | ||