Slow-release formulations of the herbicide picloram by using Fe–Al pillared montmorillonite

Slow-release formulations of the herbicide picloram (PCM, 4-amino-3,5,6-trichloropyridine-2-carboxylic acid) were designed based on its adsorption on pillared clays (pillared clays (PILCs)) for reducing the water-polluting risk derived from its use in conventional formulations. Fe–Al PILCs were synt...

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Autor principal: Marco-Brown, J.L
Otros Autores: Undabeytia, T., Torres Sánchez, R.M, dos Santos Afonso, M.
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Publicado: Springer Verlag 2017
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024 7 |2 cas  |a aluminum silicate, 12183-80-1, 1302-93-8, 1318-74-7, 1335-30-4, 61027-90-5; bentonite, 1302-78-9; picloram, 1918-02-1; Aluminum Silicates; Bentonite; clay; Herbicides; Picloram 
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100 1 |a Marco-Brown, J.L. 
245 1 0 |a Slow-release formulations of the herbicide picloram by using Fe–Al pillared montmorillonite 
260 |b Springer Verlag  |c 2017 
270 1 0 |m Marco-Brown, J.L.; Departamento de Química Inorgánica, Analítica y Química Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, Pabellón II, Argentina; email: josemarcobrown@gmail.com 
506 |2 openaire  |e Política editorial 
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520 3 |a Slow-release formulations of the herbicide picloram (PCM, 4-amino-3,5,6-trichloropyridine-2-carboxylic acid) were designed based on its adsorption on pillared clays (pillared clays (PILCs)) for reducing the water-polluting risk derived from its use in conventional formulations. Fe–Al PILCs were synthesized by the reaction of Na+-montmorillonite (SWy-2) with base-hydrolyzed solutions of Fe and Al. The Fe/(Fe + Al) ratios used were 0.15 and 0.50. The PCM adsorption isotherms on Fe–Al PILCs were well fitted to Langmuir and Freundlich models. The PCM adsorption capacity depended on the Fe content in the PILCs. Slow-release formulations were prepared by enhanced adsorption of the herbicide from PCM-cyclodextrin (CD) complexes in solution. CDs were able to enhance up to 2.5-fold the solubility of PCM by the formation of inclusion complexes where the ring moiety of the herbicide was partially trapped within the CD cavity. Competitive adsorption of anions such as sulfate, phosphate, and chloride as well as the FTIR analysis of PCM-PILC complexes provided evidence of formation of inner sphere complexes of PCM-CD on Fe–Al PILCs. Release of the herbicide in a sandy soil was lower from Fe–Al PILC formulations relative to a PCM commercial formulation. © 2017, Springer-Verlag Berlin Heidelberg.  |l eng 
536 |a Detalles de la financiación: Secretaria Nacional de Ciencia y Tecnología 
536 |a Detalles de la financiación: Ministerio de la Producción, Ciencia y Tecnología 
536 |a Detalles de la financiación: Ministerio de Educación y Cultura, CTM2013-42306-R 
536 |a Detalles de la financiación: Universidad de Buenos Aires 
536 |a Detalles de la financiación: European Social Fund, ESF 
536 |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas 
536 |a Detalles de la financiación: P12-RNM1897 
536 |a Detalles de la financiación: The authors acknowledge Universidad de Buenos Aires, Secretaria de Ciencia y T?cnica Projects, Ministerio de Ciencia y T?cnica, Agencia Nacional de Promoci?n Cient?fica y Tecnol?gica, MINCyT-ANPCyT-FONCyT, and Consejo Nacional de Investigaciones Cient?ficas y T?cnicas de la Rep?blica Argentina (CONICET) for financial support. J.L.M-B acknowledges CONICET fellowship. This research was also supported by the MEC Project CTM2013-42306-R and the Junta de Andaluc?a Project P12-RNM1897. Both projects received funding by the European Social Fund. The authors also acknowledge the Analytical Services of Seville University (CITIUS) for SEM-EDS measurements. 
593 |a Departamento de Química Inorgánica, Analítica y Química Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Ciudad Universitaria, Pabellón II, Buenos Aires, C1428EHA, Argentina 
593 |a Instituto de Química Física de los Materiales, Medio Ambiente y Energía de la Facultad de Ciencias Exactas y Naturales (INQUIMAE), CONICET-Universidad de Buenos Aires, Buenos Aires, Argentina 
593 |a Instituto de Investigación e Ingeniería Ambiental (3iA), CONICET, Escuela de Ciencia y Tecnología, UNSAM, 25 de Mayo y Francia (1650), San Martín, Argentina 
593 |a Institute of Natural Resources and Agrobiology (IRNAS-CSIC), Reina Mercedes 10. Apdo. 1052, Sevilla, 41080, Spain 
593 |a Centro de Tecnología en Recursos Minerales y Cerámica (CETMIC), CONICET-CCT La Plata-CIC, Camino Centenario y 506 CC (49), M. B. Gonnet, B1897ZCA, Argentina 
690 1 0 |a ADSORPTION 
690 1 0 |a FE–AL PILLARED MONTMORILLONITE 
690 1 0 |a PICLORAM 
690 1 0 |a SLOW-RELEASE FORMULATIONS 
690 1 0 |a ADSORPTION 
690 1 0 |a ANION 
690 1 0 |a HERBICIDE 
690 1 0 |a HYDROLYSIS 
690 1 0 |a MONTMORILLONITE 
690 1 0 |a PESTICIDE RESIDUE 
690 1 0 |a SANDY SOIL 
690 1 0 |a WATER POLLUTION 
690 1 0 |a ALUMINUM SILICATE 
690 1 0 |a BENTONITE 
690 1 0 |a CLAY 
690 1 0 |a HERBICIDE 
690 1 0 |a PICLORAM 
690 1 0 |a ADSORPTION 
690 1 0 |a ADSORPTION 
690 1 0 |a ALUMINUM SILICATES 
690 1 0 |a BENTONITE 
690 1 0 |a HERBICIDES 
690 1 0 |a PICLORAM 
700 1 |a Undabeytia, T. 
700 1 |a Torres Sánchez, R.M. 
700 1 |a dos Santos Afonso, M. 
773 0 |d Springer Verlag, 2017  |g v. 24  |h pp. 10410-10420  |k n. 11  |p Environ. Sci. Pollut. Res.  |x 09441344  |t Environmental Science and Pollution Research 
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