New insights on the structure of the picloram-montmorillonite surface complexes

Hypothesis: The environmental mobility and bioavailability of Picloram (PCM) are determined by the amine and carboxylate chemical groups interaction with the soils mineral phases. Clay particles, such as montmorillonite (Mt), and the pH value of the media could play an important role in adsorption p...

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Autor principal: Marco-Brown, J.L
Otros Autores: Trinelli, M.A, Gaigneaux, E.M, Torres Sánchez, R.M, Dos Santos Afonso, M.
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: Academic Press Inc. 2015
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Acceso en línea:Registro en Scopus
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024 7 |2 scopus  |a 2-s2.0-84921033392 
024 7 |2 cas  |a montmorillonite, 1318-93-0, 61029-13-8; picloram, 1918-02-1; aluminum silicate, 12183-80-1, 1302-93-8, 1318-74-7, 1335-30-4, 61027-90-5; bentonite, 1302-78-9; Aluminum Silicates; Bentonite; clay; Herbicides; Picloram; Soil 
040 |a Scopus  |b spa  |c AR-BaUEN  |d AR-BaUEN 
030 |a JCISA 
100 1 |a Marco-Brown, J.L. 
245 1 0 |a New insights on the structure of the picloram-montmorillonite surface complexes 
260 |b Academic Press Inc.  |c 2015 
270 1 0 |m Dos Santos Afonso, M.; Departamento de Química Inorgánica, Analítica y Química Física e INQUIMAE, FCEN, UBA, Ciudad Universitaria, Pabellón II, Argentina 
506 |2 openaire  |e Política editorial 
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520 3 |a Hypothesis: The environmental mobility and bioavailability of Picloram (PCM) are determined by the amine and carboxylate chemical groups interaction with the soils mineral phases. Clay particles, such as montmorillonite (Mt), and the pH value of the media could play an important role in adsorption processes. Thus, the study of the role of soil components other than organic matter deserves further investigation for a more accurate assessment of the risk of groundwater contamination. Experiments: Samples with PCM adsorbed on Mt dispersions were prepared at pH 3-9. Subsequently, the dispersions were separated, washed, centrifuged and stored at room temperature. Picloram (PCM) herbicide interaction with surface groups of montmorillonite (Mt) was studied using XRD, DTA, FTIR and XPS techniques. Findings: The entrance of PCM into the Mt basal space, in two different arrangements, perpendicular and planar, is proposed and the final arrangement depends on PCM concentration. The interaction of PCM with Mt surface sites through the nitrogen of the pyridine ring and carboxylic group of PCM, forming bidentate and bridge inner-sphere complexes was confirmed by FTIR and XPS analysis. The acidity constant of the PCM adsorbed on the Mt surface was calculated. © 2014 Elsevier Inc.  |l eng 
536 |a Detalles de la financiación: Agencia Nacional de Promoción Científica y Tecnológica 
536 |a Detalles de la financiación: BE/PA05-EXIII/001 
536 |a Detalles de la financiación: Universidad de Buenos Aires 
536 |a Detalles de la financiación: Ministerio de la Producción, Ciencia y Tecnología 
536 |a Detalles de la financiación: Secretaría de Ciencia y Técnica, Universidad de Buenos Aires, X043, PICT 23-32678, X067 
536 |a Detalles de la financiación: Fondo para la Investigación Científica y Tecnológica 
536 |a Detalles de la financiación: The authors acknowledge the Universidad de Buenos Aires (UBA) and Ministerio de Ciencia y Tecnología, Agencia Nacional de Promoción Científica y Tecnológica, Fondo para la Investigación Científica y Tecnológica (MINCyT-ANPCyT-FONCyT) for financial support through UBACyT X043, X067, PICT 23-32678 and SECyT/FNRS BE/PA05-EXIII/001 grants. R.M.T.S is member of CONICET and J.L.M-B and M.A.T. acknowledge CONICET fellowships. The authors also are grateful to Michel I. Genet for his assistance with XPS interpretation. Appendix A 
593 |a Departamento de Química Inorgánica, Analítica y Química Física e INQUIMAE, FCEN, UBA, Ciudad Universitaria, Pabellón II, Buenos Aires, C1428EHA, Argentina 
593 |a Université Catholique de Louvain, Institute of Condensed Matter and Nanosciences (IMCN), Division Solids, Molecules and Reactivity (MOST), Croix du Sud 2/L7.05.17, Louvain-la-Neuve, B-1348, Belgium 
593 |a CETMIC (Centro de Tecnología en Minerales y Cerámica), Camino Centenario y 506 CC (49), M. B. Gonnet, B1897ZCA, Argentina 
690 1 0 |a CLAY MINERALS 
690 1 0 |a MONTMORILLONITE 
690 1 0 |a PICLORAM HERBICIDE 
690 1 0 |a SURFACE COMPLEXES 
690 1 0 |a BIOCHEMISTRY 
690 1 0 |a CARBOXYLATION 
690 1 0 |a CLAY MINERALS 
690 1 0 |a DISPERSIONS 
690 1 0 |a GROUNDWATER 
690 1 0 |a GROUNDWATER POLLUTION 
690 1 0 |a PYRIDINE 
690 1 0 |a RISK ASSESSMENT 
690 1 0 |a WEED CONTROL 
690 1 0 |a X RAY PHOTOELECTRON SPECTROSCOPY 
690 1 0 |a ADSORPTION PROCESS 
690 1 0 |a ENVIRONMENTAL MOBILITY 
690 1 0 |a GROUNDWATER CONTAMINATION 
690 1 0 |a INNER SPHERE COMPLEXES 
690 1 0 |a MONTMORILLONITE SURFACE 
690 1 0 |a MONTMORILLONITES (MT) 
690 1 0 |a PICLORAM 
690 1 0 |a SURFACE COMPLEX 
690 1 0 |a HERBICIDES 
690 1 0 |a GROUND WATER 
690 1 0 |a MONTMORILLONITE 
690 1 0 |a ORGANIC MATTER 
690 1 0 |a PICLORAM 
690 1 0 |a ALUMINUM SILICATE 
690 1 0 |a BENTONITE 
690 1 0 |a CLAY 
690 1 0 |a HERBICIDE 
690 1 0 |a PICLORAM 
690 1 0 |a SOIL 
690 1 0 |a ACID DISSOCIATION CONSTANT 
690 1 0 |a ADSORPTION 
690 1 0 |a ARTICLE 
690 1 0 |a CLAY 
690 1 0 |a COMPLEX FORMATION 
690 1 0 |a DESORPTION 
690 1 0 |a DISPERSION 
690 1 0 |a EQUILIBRIUM CONSTANT 
690 1 0 |a POROSITY 
690 1 0 |a PRIORITY JOURNAL 
690 1 0 |a SOIL PROPERTY 
690 1 0 |a THERMOGRAVIMETRY 
690 1 0 |a WATER CONTAMINATION 
690 1 0 |a X RAY DIFFRACTION 
690 1 0 |a X RAY PHOTOELECTRON SPECTROSCOPY 
690 1 0 |a CHEMISTRY 
690 1 0 |a INFRARED SPECTROSCOPY 
690 1 0 |a SOIL 
690 1 0 |a SURFACE PROPERTY 
690 1 0 |a ADSORPTION 
690 1 0 |a ALUMINUM SILICATES 
690 1 0 |a BENTONITE 
690 1 0 |a HERBICIDES 
690 1 0 |a PHOTOELECTRON SPECTROSCOPY 
690 1 0 |a PICLORAM 
690 1 0 |a SOIL 
690 1 0 |a SPECTROSCOPY, FOURIER TRANSFORM INFRARED 
690 1 0 |a SURFACE PROPERTIES 
690 1 0 |a X-RAY DIFFRACTION 
650 1 7 |2 spines  |a PH 
700 1 |a Trinelli, M.A. 
700 1 |a Gaigneaux, E.M. 
700 1 |a Torres Sánchez, R.M. 
700 1 |a Dos Santos Afonso, M. 
773 0 |d Academic Press Inc., 2015  |g v. 444  |h pp. 115-122  |p J. Colloid Interface Sci.  |x 00219797  |w (AR-BaUEN)CENRE-15  |t Journal of Colloid and Interface Science 
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