Sorption of mixed methanol + water vapours by ion-exchange resins

The sorption of mixed water + methanol vapours by ion-exchange resins in the sodium form has been studied gravimetrically (McBain quartz spring balance) at 25 °C, using the isopiestic method (equilibrating mixture: water + methanol + glycerol) for controlling the total vapour pressure and the vapour...

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Autor principal: Crovetto, R.
Otros Autores: Timmermann, E.O
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 1982
Acceso en línea:Registro en Scopus
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100 1 |a Crovetto, R. 
245 1 0 |a Sorption of mixed methanol + water vapours by ion-exchange resins 
260 |c 1982 
270 1 0 |m Timmermann, E.O.; Instituto de Investigaciones Fisicoquimicas Teóricas y Aplicadas (INIFTA), Casilla de Correo 16, (1900) La Plata, Argentina 
506 |2 openaire  |e Política editorial 
504 |a Herlihy, J., (1968), Ph.D. Thesis (University of Washington, Seattle; Myers, A., Prausnitz, J., (1965) AICHE J., 11, p. 121 
504 |a Davies, C.W., Thomas, J.J., (1952) J. Chem. Soc., p. 1607 
504 |a Gregor, H.P., Nobel, D., Gottlieb, M.H., (1955) J. Phys. Chem., 59, p. 10 
504 |a Gable, R.W., Strobel, H.A., (1956) J. Phys. Chem., 60, p. 513 
504 |a Starobinets, G.L., Novitskaya, L.V., Sevostyanova, L.I., (1968) Russ. J. Phys. Chem., 42, p. 575 
504 |a Nandam, D., Gupta, A.R., Shandar, J., (1972) Indian J. Chem., 10, p. 83 
504 |a Hall, P.G., Müller, S.A., (1978) J. Chem. Soc., Faraday Trans. 1, 74, p. 948 
504 |a Helfferich, F., (1962) Ion Exchange, , McGraw-Hill, New York 
504 |a Kunin, K., Kun, R., (1967) J. Polym. Sci., 16, p. 1457 
504 |a Kunin, K., (1972) Amber-Hi-Lites, (127-128). , Rohm and Haas Co 
504 |a Crovetto, R., (1974), Ph.D. Thesis, Universidad de Buenos Aires, Argentina; Crovetto, R., Timmermann, E.O., (1979) An. Asoc. Quínt. Argent., 67, p. 51 
504 |a Rao, B.S., (1932) J. Phys. Chem., 36, p. 616 
504 |a Williams, A.M., (1914) Trans. Faraday Soc., 10, p. 167 
504 |a Simek, M., (1970) Collect. Czech. Chem. Commun., 35, p. 2275 
520 3 |a The sorption of mixed water + methanol vapours by ion-exchange resins in the sodium form has been studied gravimetrically (McBain quartz spring balance) at 25 °C, using the isopiestic method (equilibrating mixture: water + methanol + glycerol) for controlling the total vapour pressure and the vapour composition. The two resins selected for study, the gel-type Amberlite IR-120 and the macroporous Amberlite 200, give normal water sorption isotherms, but the gel resin shows irreproducible methanol vapour sorption. Systematic mixed sorption measurements were made on the macroporous resin, which presents a slight hysteresis loop for pure methanol vapour so that only rising experiments were performed. The results are analysed at constant total vapour pressure and at constant vapour composition. The mixed isotherms are, like the pure ones, of type II (B.E.T.) At saturation, capillary sorption between beds distorts the experimental results and a smooth extrapolation procedure is applied, which allows reliable data to be obtained for these states. In equilibrium, through the vapour phase to the liquid phase the resin shows a change of selectivity, preferring the minor component of the mixture. On the other hand, methanol is selected at constant vapour composition and decreasing total vapour pressure when using methanol-rich vapours.  |l eng 
593 |a Departamento de Química Inorgánica, Analítica y Química Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, Buenos Aires, Argentina 
593 |a Comisión Nacional de Energía Atómica, Buenos Aires, Argentina 
593 |a Instituto de Investigaciones Fisicoquimicas Teóricas y Aplicadas (INIFTA), Casilla de Correo 16, (1900) La Plata, Argentina 
700 1 |a Timmermann, E.O. 
773 0 |d 1982  |g v. 78  |h pp. 2609-2618  |k n. 9  |x 03009599  |w (AR-BaUEN)CENRE-78  |t Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases 
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856 4 0 |u https://doi.org/10.1039/F19827802609  |y DOI 
856 4 0 |u https://hdl.handle.net/20.500.12110/paper_03009599_v78_n9_p2609_Crovetto  |y Handle 
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