Determination of As(III) and total inorganic As in water samples using an on-line solid phase extraction and flow injection hydride generation atomic absorption spectrometry
A simple and robust on-line sequential injection system based on solid phase extraction (SPE) coupled to a flow injection hydride generation atomic absorption spectrometer (FI-HGAAS) with a heated quartz tube atomizer (QTA) was developed and optimized for the determination of As(III) in groundwater...
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| Lenguaje: | Inglés |
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2011
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| Acceso en línea: | Registro en Scopus DOI Handle Registro en la Biblioteca Digital |
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| LEADER | 13129caa a22015617a 4500 | ||
|---|---|---|---|
| 001 | PAPER-10673 | ||
| 003 | AR-BaUEN | ||
| 005 | 20230518204044.0 | ||
| 008 | 190411s2011 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-79952484956 | |
| 024 | 7 | |2 cas |a arsenic, 7440-38-2; bicarbonate, 144-55-8, 71-52-3; chloride, 16887-00-6; hydrochloric acid, 7647-01-0; nitrate, 14797-55-8; oxygen, 7782-44-7; sodium borohydride, 16940-66-2; sodium hydroxide, 1310-73-2; sulfate, 14808-79-8; Arsenic, 7440-38-2; Arsenicals; Water, 7732-18-5 | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 030 | |a JHMAD | ||
| 100 | 1 | |a Sigrist, M. | |
| 245 | 1 | 0 | |a Determination of As(III) and total inorganic As in water samples using an on-line solid phase extraction and flow injection hydride generation atomic absorption spectrometry |
| 260 | |c 2011 | ||
| 270 | 1 | 0 | |m Sigrist, M.; Laboratorio Central, Facultad de Ingeniería Química, Universidad Nacional del Litoral, Santiago del Estero 2654-Piso 6, (3000) Santa Fe, Argentina; email: msigrist@fiq.unl.edu.ar |
| 506 | |2 openaire |e Política editorial | ||
| 504 | |a (2001), WHO, Environmental Health Criteria 224, 2nd ed., Arsenic Compounds, World Health Organization, Geneva; Smedley, P., Kinniburgh, D., A review of the source, behavior and distribution of arsenic in natural waters (2002) Appl. Geochem., 17, pp. 517-568 | ||
| 504 | |a Mandal, B., Suzuki, K., Arsenic round the world: a review (2002) Talanta, 58, pp. 201-235 | ||
| 504 | |a Smedley, P., Edmunds, W., Pelig-Ba, K., Mobility of arsenic in groundwater in the Obuasi gold-mining area of Ghana: some implications for human health (1996) Geol. Soc., 113, pp. 163-181 | ||
| 504 | |a Chen, M., Lena, Q., Hoogeweg, C., Harris, W., Arsenic background concentrations in Florida, U.S.A. surface soils: determination and interpretation (2001) Environ. Forensics, 2, pp. 117-126 | ||
| 504 | |a Walker, M., Seiler, R., Meinert, M., Effectiveness of household reverse-osmosis systems in a Western U.S. region with high arsenic in groundwater (2008) Sci. Total Environ., 389, pp. 245-252 | ||
| 504 | |a Bednar, A., Garbarino, J., Ranville, J., Wildeman, T., Effects of iron on arsenic speciation and redox chemistry in acid mine water (2005) J. Geochem. Exploration, 85, pp. 55-62 | ||
| 504 | |a Chen, H., Frey, M., Clifford, D., McNeil, L., Edwards, M., Arsenic treatment considerations (1999) J. Am. Water Works Assoc., 91, pp. 74-85 | ||
| 504 | |a (1993), WHO, Guidelines for Drinking Water Quality, Volume 1: Recommendations, 2nd ed., World Health Organization, Geneva; (2001), US Environmental Protection Agency,National Primary Drinking Water Regulations, Arsenic and Clarifications to Compliance and New Source Contaminants Monitoring, Final Rule, 40 CFR Parts 141-142, 66(14), 6976; (1998), CE, Drinking Water Directive (DWD), Council Directive 98/83/CE; (2007), Ministerio de Salud y Acción Social de La República Argentina, Código Alimentario Argentino, Capítulo XII; Petrick, J., Ayala-Fierro, F., Cullen, W., Carter, D., Aposhian, H., Monomethylarsonous acid (MMAIII) is more toxic than arsenite in chang human hepatocytes (2000) Toxicol. Appl. Pharmacol., 163, pp. 203-207 | ||
| 504 | |a Morales, K., Ryan, L., Brown, K., Kuo, T., Wu, M., Chen, C., Risk of internal cancers from arsenic in drinking water (2000) Environ. Health Perspect., 108, pp. 655-661 | ||
| 504 | |a Clewell, H., Barton, H., Gentry, P., Shipp, A., Yager, J., Andersen, M., Requirements for a biologically realistic cancer risk assessment for inorganic arsenic (1999) Int. J. Toxicol., 18 (2), pp. 131-147 | ||
| 504 | |a Dedina, J., Tsalev, D., (1995) Hydride Generation Atomic Absorption Spectrometry, , Wiley & Sons Inc., Chichester | ||
| 504 | |a Anderson, R., Thompson, M., Culbard, E., Selective reduction of arsenic species by continuous hydride generation. Part I. Reaction media (1986) Analyst, 111, pp. 1143-1152 | ||
| 504 | |a Torralba, R., Bonilla, M., Palacios, A., Cámara, C., Flow injection analysis and continuous flow systems to determine As(III) and As(V) by hydride generation atomic absorption spectrometry (1994) Analusis, 22, pp. 478-482 | ||
| 504 | |a Coelho, N., Cósmen da Silva, A., Moraes da Silva, C., Determination of As(III) and total inorganic arsenic by flow injection hydride generation atomic absorption spectrometry (2002) Anal. Chim. Acta, 460, pp. 227-233 | ||
| 504 | |a Anthemidis, A., Zachariadis, G., Stratis, J., Determination of arsenic(III) and total inorganic arsenic in water samples using an on-line sequential insertion system and hydride generation atomic absorption spectrometry (2005) Anal. Chim. Acta, 547, pp. 237-242 | ||
| 504 | |a Sigrist, M., Beldoménico, H., Determination of inorganic arsenic species by flow injection hydride generation atomic absorption spectrometry with variable sodium tetrahydroborate concentrations (2004) Spectrochim. Acta Part B, 59, pp. 1041-1045 | ||
| 504 | |a Gonzalvez, A., Cervera, M., Armenta, S., de La Guardia, M., A review of non-chromatographic methods for speciation analysis (2009) Anal. Chim. Acta, 636, pp. 129-157 | ||
| 504 | |a Narcise, C., Coo, L., del Mundo, F., On-line preconcentration and speciation of arsenic by flow injection hydride generation atomic absorption spectrophotometry (2005) Talanta, 68, pp. 298-304 | ||
| 504 | |a Yalcin, S., Le, X.L., Low pressure chromatographic separation of inorganic arsenic species using solid phase extraction cartridges (1998) Talanta, 47, pp. 787-796 | ||
| 504 | |a Le, X., Yalcin, S., Ma, M., Speciation of submicrogram per liter levels of arsenic in water: on-site species separation integrated with sample collection (2000) Environ. Sci. Technol., 34, pp. 2342-2347 | ||
| 504 | |a Hall, G., Pelchat, J., Gauthier, G., Stability of inorganic arsenic(III) and arsenic(V) in water samples (1999) J. Anal. At. Spectrom., 14, pp. 205-231 | ||
| 504 | |a Sigrist, M., Beldoménico, H., Tudino, M., Determination of As(III) in nonacidified groundwater samples for inorganic speciation analysis using flow injection hydride generation atomic absorption spectrometry (2010) Spectrosc. Lett., 43, pp. 458-464 | ||
| 504 | |a Massart, D., Vandeginste, B., Buydens, L., De Jong, S., Lewi, P., (1997) Smeyers-Verbeke Handbook ok Chemometrics and Qualimetrics: Part A, , Elsevier, Science B.V, Amsterdam, The Netherlands, B. Vandeginste, S. Rutan (Eds.) | ||
| 504 | |a Miller, J.C., Miller, J.N., (1988) Statistics for Analytical Chemistry, , Ellis Horwood Limited, Great Britain | ||
| 504 | |a Duarte, F.A., Pereira, J.S.F., Mesko, M.F., Goldschmidt, F., Flores, E.M.M., Dressler, V.L., Evaluation of liquid chromatography inductively coupled plasma mass spectrometry for arsenic speciation in water from industrial treatment of shale (2007) Spectrochim. Acta Part B, 62, pp. 978-984 | ||
| 520 | 3 | |a A simple and robust on-line sequential injection system based on solid phase extraction (SPE) coupled to a flow injection hydride generation atomic absorption spectrometer (FI-HGAAS) with a heated quartz tube atomizer (QTA) was developed and optimized for the determination of As(III) in groundwater without any kind of sample pretreatment. The method was based on the selective retention of inorganic As(V) that was carried out by passing the filtered original sample through a cartridge containing a chloride-form strong anion exchanger. Thus the most toxic form, inorganic As(III), was determined fast and directly by AsH3 generation using 3.5molL-1 HCl as carrier solution and 0.35% (m/v) NaBH4 in 0.025% NaOH as the reductant. Since the uptake of As(V) should be interfered by several anions of natural occurrence in waters, the effect of Cl-, SO4 2-, NO3 -, HPO4 2-, HCO3 - on retention was evaluated and discussed. The total soluble inorganic arsenic concentration was determined on aliquots of filtered samples acidified with concentrated HCl and pre-reduced with 5% KI-5% C6H8O6 solution. The concentration of As(V) was calculated by difference between the total soluble inorganic arsenic and As(III) concentrations. Detection limits (LODs) of 0.5μgL-1 and 0.6μgL-1 for As(III) and inorganic total As, respectively, were obtained for a 500μL sample volume. The obtained limits of detection allowed testing the water quality according to the national and international regulations. The analytical recovery for water samples spiked with As(III) ranged between 98% and 106%. The sampling throughput for As(III) determination was 60samplesh-1. The device for groundwater sampling was especially designed for the authors. Metallic components were avoided and the contact between the sample and the atmospheric oxygen was carried to a minimum. On-field arsenic species separation was performed through the employ of a serial connection of membrane filters and anion-exchange cartridges. Advantages derived from this approach were evaluated. HPLC-ICPMS was employed to study the consistency of the analytical results. © 2011 Elsevier B.V. |l eng | |
| 536 | |a Detalles de la financiación: Universidad Nacional del Litoral | ||
| 536 | |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas | ||
| 536 | |a Detalles de la financiación: The authors are grateful to Dr. Erico Marlon de Moraes Flores of Department of Chemistry, Universidade Federal de Santa María, Brazil, for his valuable collaboration in the comparison of results by HPLC–ICP–MS. They also acknowledge UBA , UNL and CONICET for financial support. | ||
| 593 | |a Laboratorio Central, Facultad de Ingeniería Química, Universidad Nacional del Litoral, Santiago del Estero 2654-Piso 6, (3000) Santa Fe, Argentina | ||
| 593 | |a Laboratorio de Análisis de Trazas, Departamento de Química Inorgánica, Analítica y Química Física/INQUIMAE, Facultad de Ciencias Exactas y Naturales, Pabellón II, Ciudad Universitaria (1428), Buenos Aires, Argentina | ||
| 690 | 1 | 0 | |a AAS |
| 690 | 1 | 0 | |a ARSENIC SPECIATION |
| 690 | 1 | 0 | |a FLOW INJECTION |
| 690 | 1 | 0 | |a HYDRIDE GENERATION |
| 690 | 1 | 0 | |a ON-LINE SEPARATION |
| 690 | 1 | 0 | |a AAS |
| 690 | 1 | 0 | |a ARSENIC SPECIATION |
| 690 | 1 | 0 | |a FLOW INJECTION |
| 690 | 1 | 0 | |a HYDRIDE GENERATION |
| 690 | 1 | 0 | |a ON-LINE SEPARATION |
| 690 | 1 | 0 | |a ABSORPTION SPECTROSCOPY |
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| 690 | 1 | 0 | |a ATOMIC ABSORPTION SPECTROMETRY |
| 690 | 1 | 0 | |a CHLORINE COMPOUNDS |
| 690 | 1 | 0 | |a EFFLUENT TREATMENT |
| 690 | 1 | 0 | |a GROUNDWATER |
| 690 | 1 | 0 | |a HYDROCHLORIC ACID |
| 690 | 1 | 0 | |a INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY |
| 690 | 1 | 0 | |a MASS SPECTROMETERS |
| 690 | 1 | 0 | |a NEGATIVE IONS |
| 690 | 1 | 0 | |a OPTIMIZATION |
| 690 | 1 | 0 | |a OXYGEN |
| 690 | 1 | 0 | |a POTASSIUM IODIDE |
| 690 | 1 | 0 | |a PROJECTILES |
| 690 | 1 | 0 | |a QUARTZ |
| 690 | 1 | 0 | |a WATER ABSORPTION |
| 690 | 1 | 0 | |a WATER INJECTION |
| 690 | 1 | 0 | |a WATER POLLUTION |
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| 690 | 1 | 0 | |a BICARBONATE |
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| 690 | 1 | 0 | |a GROUNDWATER RESOURCE |
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| 690 | 1 | 0 | |a SPECIATION (CHEMISTRY) |
| 690 | 1 | 0 | |a SPECTROMETRY |
| 690 | 1 | 0 | |a SULFATE |
| 690 | 1 | 0 | |a WATER QUALITY |
| 690 | 1 | 0 | |a ACIDIFICATION |
| 690 | 1 | 0 | |a ANION EXCHANGE |
| 690 | 1 | 0 | |a ARTICLE |
| 690 | 1 | 0 | |a ATOMIC ABSORPTION SPECTROMETRY |
| 690 | 1 | 0 | |a FLOW INJECTION ANALYSIS |
| 690 | 1 | 0 | |a HIGH PERFORMANCE LIQUID CHROMATOGRAPHY |
| 690 | 1 | 0 | |a MASS SPECTROMETRY |
| 690 | 1 | 0 | |a SOLID PHASE EXTRACTION |
| 690 | 1 | 0 | |a WATER ANALYSIS |
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| 690 | 1 | 0 | |a EQUIPMENT DESIGN |
| 690 | 1 | 0 | |a LIMIT OF DETECTION |
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| 690 | 1 | 0 | |a SPECTROPHOTOMETRY, ATOMIC |
| 690 | 1 | 0 | |a WATER |
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| 650 | 1 | 7 | |2 spines |a PH |
| 700 | 1 | |a Albertengo, A. | |
| 700 | 1 | |a Beldoménico, H. | |
| 700 | 1 | |a Tudino, M. | |
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