Influence of the microstructure of vulcanized polybutadiene rubber on the dielectric properties

Dielectric relaxation spectra in the frequency range from 10 Hz to 1 GHz were obtained at room temperature to study the influence of the network structure formed during vulcanization on the dielectric properties of polybutadiene rubber (BR). Two polybutadiene rubbers with different cis, trans and vi...

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Autor principal: Rodríguez Garraza, Ana Lucía
Otros Autores: Sorichetti, Patricio Aníbal, Marzocca, Angel José, Matteo, Claudia Leda, Monti, G.A
Formato: Capítulo de libro
Lenguaje:Inglés
Publicado: 2011
Acceso en línea:Registro en Scopus
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100 1 |a Rodríguez Garraza, Ana Lucía 
245 1 0 |a Influence of the microstructure of vulcanized polybutadiene rubber on the dielectric properties 
260 |c 2011 
270 1 0 |m Marzocca, A.J.; Departamento de Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, C1428EGA Buenos Aires, Argentina; email: marzo@df.uba.ar 
504 |a Arbe, A., Richter, D., Colmenero, J., Farago, B., Merging of the α and β relaxations in polybutadiene: A neutron spin echo and dielectric study (1996) Phys. Rev. e, 54, pp. 3853-3869 
504 |a Hofmann, A., Alegria, A., Colmenero, J., Willner, L., Buscaglia, E., Hadjichristidis, N., Secondary and segmental relaxation in polybutadienes of varying microstructure: Dielectric relaxation results (1996) Macromolecules, 29 (1), pp. 129-134 
504 |a Runt, J.P., Fitzgerald, J.J., (1997) Dielectric Spectroscopy of Polymeric Materials: Fundamentals and Applications, , American Chemical Society Washington DC 
504 |a Marzocca, A.J., Rodriguez Garraza, A.L., Sorichetti, P., Mosca, H.O., Cure kinetics and swelling behaviour in polybutadiene rubber (2010) Polym. Test., 29, pp. 477-482 
504 |a Marzocca, A.J., Rodriguez Garraza, A.L., Mansilla, M.A., Evaluation of the polymer-solvent interaction parameter χ for the system cured polybutadiene rubber and toluene (2010) Polym. Test., 29, pp. 119-126 
504 |a Sorichetti, P.A., Matteo, C.L., Low-frequency dielectric measurements of complex fluids using high-frequency coaxial sample cells (2007) Measurement: Journal of the International Measurement Confederation, 40 (4), pp. 437-449. , DOI 10.1016/j.measurement.2006.06.005, PII S0263224106001217 
504 |a Von Hippel, A.R., (1966) Dielectric Materials and Applications, , MIT Press Cambridge, Massachusetts (Chapter 4) 
504 |a Havriliak, S., Negami, S., A complex plane analysis of α-dispersions in some polymer systems (1966) J.Polym.Sci., Polym. Symp., 14, pp. 99-117 
504 |a Vogel, H., Das Temperaturabhaengigkeitsgesetz der (1921) Viskositaet von Fluessigkeiten Phys. Z., 22, p. 645 
504 |a Fulcher, G.S., Analysis of recent measurements of the viscosity of glasses (1925) J. Am. Ceramic Soc., 8, pp. 339-355 
504 |a Clough, R.S., Koenig, J.L., Solid-state carbon-13 NMR studies of vulcanized elastomers. VII. Sulfur-vulcanized CIS-1,4-polybutadiene at 75.5 MHz (1989) Rubber Chemistry and Technology, 62 (5), pp. 908-927 
504 |a Smith, S.R., Koenig, J.L., Solid-state carbon-13 NMR studies of vulcanized elastomers. IX: TMTD-vulcanized cis-1,4-polybutadiene at 75.5 MHz (1992) Rubber Chem. Technol., 65, pp. 176-200 
506 |2 openaire  |e Política editorial 
520 3 |a Dielectric relaxation spectra in the frequency range from 10 Hz to 1 GHz were obtained at room temperature to study the influence of the network structure formed during vulcanization on the dielectric properties of polybutadiene rubber (BR). Two polybutadiene rubbers with different cis, trans and vinyl content in their molecular structure were used to prepare compounds with a cure system based on sulphur and TBBS (N-t-butyl-2-benzothiazole sulfenamide). Samples of each compound were vulcanized at 433 K for several times in order to obtain different crosslink densities. Structural changes in both compounds during vulcanization were measured by means of solid-state C-13 NMR spectroscopy. Dielectric permittivity was measured as function of the frequency and analyzed using the Havriliak-Negami model. The results show a clear dependence of the dielectric parameters on the crosslink density and 1,4-cis content. © 2011 Elsevier Ltd. All rights reserved.  |l eng 
536 |a Detalles de la financiación: Universidad de Buenos Aires, 2010–2012 
536 |a Detalles de la financiación: Consejo Nacional de Investigaciones Científicas y Técnicas, PIP 2098 
536 |a Detalles de la financiación: This work was supported by the Universidad de Buenos Aires , Argentina (Research Project 2010–2012) and CONICET (Research Project PIP 2098, 2009–2011). 
593 |a Departamento de Física, Facultad de Ciencias Exactas y Naturales, Universidad de Buenos Aires, C1428EGA Buenos Aires, Argentina 
593 |a Universidad de Buenos Aires, Facultad de Ingeniería, Departamento de Física, Av. Paseo Colón 850, Buenos Aires C1063ACV, Argentina 
593 |a CONICET, Argentina 
593 |a FaMAF, Universidad Nacional de Córdoba, Ciudad Universitaria, 5016 Córdoba, Argentina 
690 1 0 |a CROSSLINKING 
690 1 0 |a DIELECTRIC PROPERTIES 
690 1 0 |a POLYBUTADIENE RUBBER 
690 1 0 |a CROSS-LINK DENSITIES 
690 1 0 |a CU-RE SYSTEM 
690 1 0 |a DIELECTRIC PARAMETERS 
690 1 0 |a DIELECTRIC PERMITTIVITIES 
690 1 0 |a DIELECTRIC RELAXATION SPECTRA 
690 1 0 |a FREQUENCY RANGES 
690 1 0 |a HAVRILIAK-NEGAMI MODEL 
690 1 0 |a NETWORK STRUCTURES 
690 1 0 |a POLYBUTADIENE RUBBER 
690 1 0 |a POLYBUTADIENE RUBBERS 
690 1 0 |a ROOM TEMPERATURE 
690 1 0 |a STRUCTURAL CHANGE 
690 1 0 |a SULFENAMIDES 
690 1 0 |a DIELECTRIC RELAXATION 
690 1 0 |a NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY 
690 1 0 |a PERMITTIVITY 
690 1 0 |a RUBBER 
690 1 0 |a SULFUR 
690 1 0 |a VULCANIZATION 
690 1 0 |a POLYBUTADIENES 
700 1 |a Sorichetti, Patricio Aníbal 
700 1 |a Marzocca, Angel José 
700 1 |a Matteo, Claudia Leda 
700 1 |a Monti, G.A. 
773 0 |d 2011  |g v. 30  |h pp. 657-662  |k n. 6  |p Polym Test  |x 01429418  |w (AR-BaUEN)CENRE-6542  |t Polymer Testing 
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