Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine
The preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine was accomplished by oxydation of the unlabelled compound to tomatidone, exchange of the labile hydrogens by reaction with H20 and 3H2O on basic alumina and direct reduction of the labelled tomatidone to tomatidine. The efficiency of the procedure...
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| Formato: | Capítulo de libro |
| Lenguaje: | Inglés |
| Publicado: |
1986
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| Acceso en línea: | Registro en Scopus DOI Handle Registro en la Biblioteca Digital |
| Aporte de: | Registro referencial: Solicitar el recurso aquí |
| LEADER | 03284caa a22005297a 4500 | ||
|---|---|---|---|
| 001 | PAPER-1000 | ||
| 003 | AR-BaUEN | ||
| 005 | 20230607132233.0 | ||
| 008 | 190411s1986 xx ||||fo|||| 00| 0 eng|d | ||
| 024 | 7 | |2 scopus |a 2-s2.0-0022644025 | |
| 040 | |a Scopus |b spa |c AR-BaUEN |d AR-BaUEN | ||
| 100 | 1 | |a Doller, D. | |
| 245 | 1 | 0 | |a Preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine |
| 260 | |c 1986 | ||
| 270 | 1 | 0 | |m Doller, D.; Departamento de Quimica Orgànica Y Umymfor, Facultad de Ciencias Exactas Y Naturales, Universidad de Buenos Aires, Pabellón 2, Ciudad Universitaria, Buenos Aires, 1428, Argentina |
| 506 | |2 openaire |e Política editorial | ||
| 504 | |a Russo, C.A., Gros, E.G., (1981) Phytochemistry, 20, p. 1763 | ||
| 504 | |a Ghini, A.A., Burton, G., Gros, E.G., (1982) Phytochemistry, 21, p. 605 | ||
| 504 | |a Russo, C.A., Gros, E.G., (1982) Phytochemistry, 21, p. 609 | ||
| 504 | |a Russo, C.A., Burton, G., Gros, E.G., (1983) Phytochemistry, 22, p. 71 | ||
| 504 | |a Russo, C.A., Gros, E.G., (1983) Phytochemistry, 22, p. 1839 | ||
| 504 | |a Albright, I.D., (1974) J. Org. Chem., 39, p. 1977 | ||
| 504 | |a Klein, P.D., Knight, J.D., (1965) J. Am. Chem. Soc., 87, p. 2657 | ||
| 504 | |a Adam, G., Huang, H.Th., (1980) Tetrahedron Lett., 21, p. 1931 | ||
| 504 | |a Schreiber, K., Adam, G., (1961) Experientia, 17, p. 13 | ||
| 504 | |a Toldy, L., (1958) Acta. Chim. Acad. Sci Hung., 16, p. 403 | ||
| 504 | |a Bukovits, G.J., Daller, D., ; Uhle, F.C., (1961) J. Am. Chem. Soc., 83, p. 1460 | ||
| 520 | 3 | |a The preparation of |2,4‐2H|‐ and |2,4‐3H|‐tomatidine was accomplished by oxydation of the unlabelled compound to tomatidone, exchange of the labile hydrogens by reaction with H20 and 3H2O on basic alumina and direct reduction of the labelled tomatidone to tomatidine. The efficiency of the procedure was checked by physical (1H and 13C NMR, MS) methods. Copyright © 1986 John Wiley & Sons, Ltd. |l eng | |
| 593 | |a Departamento de Quimica Orgànica Y Umymfor, Facultad de Ciencias Exactas Y Naturales, Universidad de Buenos Aires, Pabellón 2, Ciudad Universitaria, Buenos Aires, 1428, Argentina | ||
| 690 | 1 | 0 | |a |2,4‐2H|‐TOMATIDINE |
| 690 | 1 | 0 | |a |2,4‐3H|‐TOMATIDINE |
| 690 | 1 | 0 | |a RADIOISOTOPE |
| 690 | 1 | 0 | |a METHODOLOGY |
| 690 | 1 | 0 | |a NONHUMAN |
| 690 | 1 | 0 | |a PRIORITY JOURNAL |
| 690 | 1 | 0 | |a THEORETICAL STUDY |
| 690 | 1 | 0 | |a TOMATIDINE H 2 |
| 690 | 1 | 0 | |a TOMATIDINE H 3 |
| 700 | 1 | |a Gros, E.G. | |
| 773 | 0 | |d 1986 |g v. 23 |h pp. 109-112 |k n. 1 |p J. Label. Compd. Radiopharm. |x 03624803 |w (AR-BaUEN)CENRE-1949 |t Journal of Labelled Compounds and Radiopharmaceuticals | |
| 856 | 4 | 1 | |u https://www.scopus.com/inward/record.uri?eid=2-s2.0-0022644025&doi=10.1002%2fjlcr.2580230114&partnerID=40&md5=09b022a28b250d97466e373af92aa7c1 |y Registro en Scopus |
| 856 | 4 | 0 | |u https://doi.org/10.1002/jlcr.2580230114 |y DOI |
| 856 | 4 | 0 | |u https://hdl.handle.net/20.500.12110/paper_03624803_v23_n1_p109_Doller |y Handle |
| 856 | 4 | 0 | |u https://bibliotecadigital.exactas.uba.ar/collection/paper/document/paper_03624803_v23_n1_p109_Doller |y Registro en la Biblioteca Digital |
| 961 | |a paper_03624803_v23_n1_p109_Doller |b paper |c PE | ||
| 962 | |a info:eu-repo/semantics/article |a info:ar-repo/semantics/artículo |b info:eu-repo/semantics/publishedVersion | ||
| 999 | |c 61953 | ||