Related substances test and characterization of seratrodast in bulk drugs

A reversed-phase high-performance liquid chromatographic (RP-HPLC) method for related substances test of seratrodast in bulk drugs has been developed. The separation was achieved on a ZirChrom Kromasil C<sub>18</sub> (200 mm×4.6 mm, 5 µm) column thermostated at 30 ºC using acetonitrile...

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Autores principales: Xu, Jufang, Hu, Yuzhu
Formato: Articulo
Lenguaje:Inglés
Publicado: 2011
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Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/8101
http://www.latamjpharm.org/resumenes/30/1/LAJOP_30_1_1_8.pdf
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Sumario:A reversed-phase high-performance liquid chromatographic (RP-HPLC) method for related substances test of seratrodast in bulk drugs has been developed. The separation was achieved on a ZirChrom Kromasil C<sub>18</sub> (200 mm×4.6 mm, 5 µm) column thermostated at 30 ºC using acetonitrile-0.05 M pH 3.0 potassium dihydrogen orthophosphate buffer (60:40, v/v) as a mobile phase. Wavelength was set at 267 nm. An external standard method using a dilution of the sample solution as reference was used for the purity test. The method was found to be simple, rapid, specific and sensitive with detection limit of 0.67 ng. A thorough study has been undertaken to identify and characterize an unknown impurity at a level over the identification threshold of 0.1 %, and its structure was elucidated as 7-(3,5,6-trimethyl-1,4-benzoquinone- 2-yl)-7-p-tolyl-heptanoic acid based on the data of MS, UV, IR and NMR spectra. Formation of the unknown impurity as well as the countermeasure was also discussed