Assignments of <sup>1</sup>H and <sup>13</sup>C resonante signals in 2-Methoxy-4,5-Methylenedioxypropiophenone with the assistance of 1D and 2D NMR experiments

In connection with our continuous investigation of Piper species, we have isolated 2-methoxy- 4,5-methylenedioxypropiophenone from the roots of Piper murginatum. The literature reported the same compound isolated from leaves of the same species, but only <sup>1</sup>H NMR (60 MHz), UV, I...

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Autores principales: Oliveira Santos, Bárbara Viviana de, Oliveira Chaves, María Célia de
Formato: Articulo
Lenguaje:Inglés
Publicado: 2000
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Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/6898
http://www.latamjpharm.org/trabajos/19/1/LAJOP_19_1_1_8_76AO009DI0.pdf
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Sumario:In connection with our continuous investigation of Piper species, we have isolated 2-methoxy- 4,5-methylenedioxypropiophenone from the roots of Piper murginatum. The literature reported the same compound isolated from leaves of the same species, but only <sup>1</sup>H NMR (60 MHz), UV, IV and EM were used in spectroscopic assignments. In the present paper we assign unambiguously the protons and carbons peaks with the assistance of 1D and 2D NMR experiments.