Mössbauer and susceptibility studies of FeMoVO<SUB>7</SUB>

The oxidic phase FeMoVO7 of the Fe2O3-V2O5-MoO3 system has been synthesized. Susceptibility measurements from 4.2 K to room temperature display an antiferromagnetic behaviour with an effective magnetic moment of 5.80ώb. This value, and the measured Mossbauer isomer shift of 0.40±0.02 mm/s, are chara...

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Autores principales: Goya, Gerardo Fabián, Mercader, Roberto Carlos, Vassallo, Marta Beatriz, Botto, Irma Lía, Sáez Puche, R.
Formato: Articulo
Lenguaje:Inglés
Publicado: 1994
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Acceso en línea:http://sedici.unlp.edu.ar/handle/10915/134552
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Sumario:The oxidic phase FeMoVO7 of the Fe2O3-V2O5-MoO3 system has been synthesized. Susceptibility measurements from 4.2 K to room temperature display an antiferromagnetic behaviour with an effective magnetic moment of 5.80ώb. This value, and the measured Mossbauer isomer shift of 0.40±0.02 mm/s, are characteristic of high-spin Fe(III). The lowTn value of 15 K suggests a weak interaction among the Fe-O polyhedra. The relative small QS=0.28±0.02 mm/s found in this compound shows that the Fe-O polyhedra symmetry is close to octahedral and almost undistorted.